Article(id=1319986962493194821, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986924727677753, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20211100, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1639584000000, receivedDateStr=2021-12-16, revisedDate=1640880000000, revisedDateStr=2021-12-31, acceptedDate=null, acceptedDateStr=null, onlineDate=1792639016030, onlineDateStr=2026-10-22, pubDate=1650384000000, pubDateStr=2022-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792639016030, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792639016030, creator=13701087609, updateTime=1792639016030, updator=13701087609, issue=Issue{id=1319986924727677753, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='4', pageStart='877', pageEnd='1200', issueExtLink='null', onlineDate='null', pubDate='1650384000000', pubDateStr='2022-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792639007026, creator='13701087609', updateTime=1792639269665, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319988026600702366, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986924727677753, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319988026600702367, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986924727677753, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=913, endPage=918, ext={EN=ArticleExt(id=1319986962719687238, articleId=1319986962493194821, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Structural Investigations of Sol-Gel Prepared Bi₂O₃-AlPO₄-SiO₂ Glasses by Solid State Nuclei Magnetic Resonance Spectroscopy, columnId=1321891873954837352, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on United Nations International Year of Glass—Research Articles, runingTitle=null, highlight=null, articleAbstract=

A series of xBi₂O₃-AlPO₄-SiO₂ glasses (0≤x≤0.15) were prepared by a sol-gel process. The local structures of glasses were investigated by magic angle spinning nuclei magnetic resonance (MAS NMR) and X-ray photoelectron spectroscopy (XPS). Based on the ²⁷Al MAS NMR spectra. The results show that trere is Bi-O-Bi connectivity in all these glasses. In addition, the prepared glass is composed of AlPO₄- and SiO₂-nanodomains according to the results of ²⁷Al{³¹P} REDOR, ³¹P{²⁷Al} REAPDOR, ³¹P CT-DRENAR-BABA-xy16, and ²⁹Si MAS NMR. The addition of Bi₂O₃ promotes the increase of AlPO₄ clusters, forming the final phase, and Bi₂O₃ exists both in SiO₂ and AlPO₄ nanodomains.

, authors=Ruili ZHANG, Jianrong WANG, Delong MA, authorsList=Ruili ZHANG, Jianrong WANG, Delong MA, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319986962988122695, articleId=1319986962493194821, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Bi₂O₃-AlPO₄-SiO₂溶胶-凝胶玻璃的制备及固体核磁共振结构解析, columnId=1321891874147775337, journalTitle=硅酸盐学报, columnName=“联合国国际玻璃年”特刊—研究论文, runingTitle=null, highlight=null, articleAbstract=

针对铋掺杂玻璃发光机理不明确的问题，以Bi₂O₃-AlPO₄-SiO₂玻璃为研究对象，对其开展结构研究。采用硝酸铋、乳酸铝、磷酸三乙酯和正硅酸四乙酯作为前驱体，通过溶胶-凝胶法制备了xBi₂O₃-AlPO₄-SiO₂（0≤x≤0.15）的三元体系玻璃，并使用固态核磁共振（NMR）技术及X射线光电子能谱系统解析了xBi₂O₃-AlPO₄-SiO₂玻璃的原子级结构。NMR结果证明：制备的玻璃由AlPO₄和SiO₂纳米团簇组成。XPS结果表明该系列的玻璃中没有形成Bi—O—Bi键。通过²⁷Al{³¹P} REDOR、³¹P{²⁷Al} REAPDOR，³¹P CT-DRENAR-BABA-xy16，及²⁹Si MAS单共振实验证明：Bi₂O₃的加入促进了AlPO₄团簇逐步增大，直到最后形成明显的分相，Bi₂O₃同时存在于SiO₂和AlPO₄两相中。

, authors=张瑞丽, 王建荣, 马德龙, authorsList=张瑞丽, 王建荣, 马德龙, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=YkKTfehcRmeBsCfjJF2JAg==, magXml=sxJU6ZssQzRbCrnDIvi1OQ==, pdfUrl=null, pdf=eK7fdWG3tHL1YYk0ZdQhEA==, pdfFileSize=1075953, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=cRPXnhMYlPoyP9RvuohvEg==, mapNumber=null, fund=null)}, authors=[Author(id=1322507105580462213, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1319986962493194821, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=mse_zhangrl@ujn.edu.cn, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1322507105681125511, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1319986962493194821, authorId=1322507105580462213, language=EN, stringName=Ruili ZHANG, firstName=Ruili, middleName=null, lastName=ZHANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=School of Material Science and Engineering, University of Jinan, Jinan 250022, China, bio={"content":"

ZHANG Ruili (1986-), female, Ph.D., Lecturer. E-mail: mse_zhangrl@ujn.edu.cn

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ZHANG Ruili (1986-), female, Ph.D., Lecturer. E-mail: mse_zhangrl@ujn.edu.cn

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张瑞丽（1986—），女，博士，讲师。

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张瑞丽（1986—），女，博士，讲师。

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