Article(id=1319986590844309909, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210902, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1634745600000, receivedDateStr=2021-10-21, revisedDate=1636300800000, revisedDateStr=2021-11-08, acceptedDate=null, acceptedDateStr=null, onlineDate=1792638927422, onlineDateStr=2026-10-22, pubDate=1655654400000, pubDateStr=2022-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792638927422, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792638927422, creator=13701087609, updateTime=1792638927422, updator=13701087609, issue=Issue{id=1319986532933555119, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='6', pageStart='1455', pageEnd='1774', issueExtLink='null', onlineDate='null', pubDate='1655654400000', pubDateStr='2022-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792638913615, creator='13701087609', updateTime=1792639299444, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319988151507075566, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319988151507075567, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1626, endPage=1633, ext={EN=ArticleExt(id=1319986591049830806, articleId=1319986590844309909, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Calcium-Silicon Molar Ratio on Early Strength Enhancement of Nano-sized Calcium Silicate Hydrate Seeds, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Nano-sized C-S-H crystal seed nucleating agent can effectively promote the hydration process of cement and improve the early strength of cementitious composites via providing some nucleation sites for cement hydration products. The calcium-silica molar ratio can affect the early strength effect of nano-sized C-S-H crystalline seeds on cement, but the specific influence law is still controversial. In this paper, the effect of calcium-silica molar ratio on the size and morphology of nano-sized C-S-H crystalline species and their early strength effects on cement was investigated by X-ray fluorescence spectroscopy, multiple light scattering analysis, dynamic light scattering analysis, X-ray diffraction, transmission electron microscopy, cement hydration exotherm and strength tests, and the mechanism of calcium-silica molar ratio affecting the early strength of nano-sized C-S-H crystalline species on cement was elucidated. The results show that the nucleation efficiency of C-S-H nano-crystals can be improved as calcium and silicon molarity is increased.The size of C-S-H nano-crystals gradually becomes smaller and the dispersion stability of suspension improves when calcium-silica molar ratio increases from 1.0 to 1.7. Also, the morphology of C-S-H nano-crystals changes from spherical to tin foil, and the stacking between the crystals decreases and the layer thickness becomes thinner when calcium-silica molar ratio increases. The C-S-H nano-crystals can promote the development of cement hydration exothermic rate and early strength, especially within the age of 1 d. The higher the calcium-silica molar ratio is, the greater the acceleration of cement hydration exothermic rate by C-S-H nano-crystals and the higher the early compressive strength enhancement will be.

, authors=Ruifeng TANG¹, Suping CUI¹, Ziming WANG¹, Zhaojia WANG^{1, 2}, Jiale ZHANG¹, Mingzhang LAN¹, authorsList=Ruifeng TANG, Suping CUI, Ziming WANG, Zhaojia WANG, Jiale ZHANG, Mingzhang LAN, authorCompany=null, correspAuthors=Suping CUI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319986591335043479, articleId=1319986590844309909, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=钙硅摩尔比对纳米水化硅酸钙晶种早强作用的影响及机理, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

纳米C-S-H晶种成核剂通过为水泥水化产物提供成核位点，能有效促进水泥水化进程，提高水泥基复合材料早期强度。研究表明，钙硅摩尔比的变化会影响纳米C-S-H晶种对水泥的早强作用，但具体影响规律尚存争议。本工作通过X射线荧光光谱分析、多重光散射分析、动态光散射分析、X射线衍射分析、透射电子显微镜、水泥水化放热及强度测试研究了钙硅摩尔比对纳米C-S-H晶种尺寸、形貌及其对水泥早强效果的影响，以阐明钙硅摩尔比对纳米C-S-H晶种早强作用的影响规律及作用机理。这对提高纳米C-S-H晶种成核效率，优化纳米C-S-H的制备工艺，推进纳米C-S-H晶种材料的工业化应用具有重要意义。结果表明：随着钙硅摩尔比在1.0~1.7的范围内的增大，纳米C-S-H悬浮液分散稳定性逐渐提高，纳米晶粒越不易团聚；同时，随着钙硅摩尔比的增大，纳米C-S-H逐渐由球状变为锡箔状，颗粒间的堆叠逐渐减小，层厚变薄。纳米C-S-H能显著促进水泥水化放热速率和早期强度的发展，尤其是1 d龄期之内的强度。钙硅摩尔比越高，纳米C-S-H对水泥水化放热速率加快的幅度越大，早期抗压强度提升的幅度越高。

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