Article(id=1319232619984834636, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210865, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1633622400000, receivedDateStr=2021-10-08, revisedDate=1636041600000, revisedDateStr=2021-11-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1792459166760, onlineDateStr=2026-10-20, pubDate=1658246400000, pubDateStr=2022-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792459166760, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792459166760, creator=13701087609, updateTime=1792459166760, updator=13701087609, issue=Issue{id=1319232566922695375, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='7', pageStart='1775', pageEnd='2066', issueExtLink='null', onlineDate='null', pubDate='1658246400000', pubDateStr='2022-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792459154109, creator='13701087609', updateTime=1792460038980, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319236278420357264, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319236278420357265, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319232566922695375, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1936, endPage=1944, ext={EN=ArticleExt(id=1319232620181966925, articleId=1319232619984834636, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Photocatalytic Performance of Copper Zinc Tin Sulfide via Hydrothermal Synthesis, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Cu₂ZnSnS₄ has good photocatalytic application prospects due to its high absorption coefficient in a visible light range and high carrier mobility, but the limited photocatalytic activity and catalytic stability restricts its practical applications. Cu₂ZnSnS₄ nanomaterial was prepared by a hydrothermal method with zinc chloride, tin chloride, copper chloride and thiourea as precursors, and PEG400 and OP10 as surfactants. The microstructure of the as-prepared Cu₂ZnSnS₄ nanomaterial was characterized and the influence of surfactant on the optical band gap and the photocatalytic degradation performance of the samples was determined by X-ray diffraction, Raman spectroscopy, X-ray photoelectron spectroscopy, scanning electron microscopy, and transmission electron microscopy, respectively. The results show that three kinds of Cu₂ZnSnS₄ materials prepared all have a kesterite micro-phase, and the addition of PEG400 and OP10 into the precursor results in the variation of the microstructure, stoichiometric ratio and optical band gap of the materials, consequently determining their photocatalytic properties. After methylene blue degradation for 50 min, Cu₂ZnSnS₄ nano-powder synthesized with PEG400 has an optimum photocatalytic degradation rate (i.e., 95.7%). It is indicated that the photocatalytic activity and stability of Cu₂ZnSnS₄ nanomaterials can be improved by reducing the optical bandgap and enhancing the crystallinity, thus paving a promising approach to improve its photocatalytic performance.

, authors=Xuemei HU¹, Junqiang QIAO^{1, 2}, authorsList=Xuemei HU, Junqiang QIAO, authorCompany=null, correspAuthors=Junqiang QIAO, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319232620584620110, articleId=1319232619984834636, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=水热法制备铜锌锡硫纳米材料及其光催化性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

铜锌锡硫（Cu₂ZnSnS₄）在可见光范围内光吸收系数高且具有良好的载流子迁移率，使其在光催化领域表现出了较好的应用前景。然而在实际应用中，其光催化活性及催化稳定性还需进一步提升。以氯化锌、氯化锡、氯化铜、硫脲为水热反应前驱体，添加PEG400、OP10为表面活性剂，通过水热反应制备Cu₂ZnSnS₄（CZTS）纳米粉体；使用X射线衍射、Raman光谱、X射线光电子能谱、扫描电子显微镜、透射电子显微镜等手段表征所制备铜锌锡硫材料微观结构，并研究在水热法制备过程中添加不同表面活性剂对所制备Cu₂ZnSnS₄纳米粉体的光学带隙和光催化性能的影响。结果表明：所制备铜锌锡硫材料均具有锌黄锡矿相结构；水热法制备铜锌锡硫纳米粉体反应前驱体中添加PEG400和OP10可有效调控铜锌锡硫纳米粉体的微观结构、化学元素计量比及光学带隙，进而改变纳米粉体的光催化性能。添加PEG400后制备得到Cu₂ZnSnS₄在50 min内光催化降解亚甲基蓝的降解率可达到95.7%，具有最优的光催化性能。减小光学带隙和提升结晶性是改善CZTS材料光催化活性及稳定性的有效途径，为提高Cu₂ZnSnS₄材料的光催化性能提供了新的思路。

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HU Xuemei (1991-), female, Assistant Professor. E-mail: xmhu@gsas.ac.cn

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HU Xuemei (1991-), female, Assistant Professor. E-mail: xmhu@gsas.ac.cn

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虎学梅（1991—），女，助理研究员。

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虎学梅（1991—），女，助理研究员。

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