Article(id=1319986556471984288, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210857, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1633708800000, receivedDateStr=2021-10-09, revisedDate=1638806400000, revisedDateStr=2021-12-07, acceptedDate=null, acceptedDateStr=null, onlineDate=1792638919226, onlineDateStr=2026-10-22, pubDate=1655654400000, pubDateStr=2022-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792638919226, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792638919226, creator=13701087609, updateTime=1792638919226, updator=13701087609, issue=Issue{id=1319986532933555119, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='6', pageStart='1455', pageEnd='1774', issueExtLink='null', onlineDate='null', pubDate='1655654400000', pubDateStr='2022-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792638913615, creator='13701087609', updateTime=1792639299444, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319988151507075566, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319988151507075567, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986532933555119, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1557, endPage=1565, ext={EN=ArticleExt(id=1319986558225203361, articleId=1319986556471984288, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Fe-Cr-Ni-Mn Black Ceramic Pigment from Stainless Steelmaking Dust, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The rich transition metal elements in stainless steelmaking dust, such as Fe, Cr, Ni, and Mn, can be used to prepare black ceramic pigments. The stainless steelmaking dust can be ultilized to prepare cobalt-free black ceramic pigments. According to the color mechanism of Fe-Cr-Ni-Mn black pigment, an appropriate amount of chemical reagents Fe₂O₃, Cr₂O₃, MnO and NiO was added into stainless steel making dust in a mixed mass ratio of 6∶1∶1∶1. The chromaticity value vibration rules of black ceramic pigments prepared under different conditions were investigated, and the coloring mechanism of the pigments was discussed as well. The results show that a high firing temperature or a long holding time causes the decomposition of Cr-containing spinel phase, adversely affecting the coloring properties of the pigment. The optimum firing process of the pigment is the firing temperature of 1 175 ℃, the holding time of 30 min, and the furnace cooling method. The L*, a* and b* values of the prepared pigment are 37.20, 0.13 and 0.02, respectively, and the main phases in the pigment are Fe₂O₃ and mixed spinels. The absorbance of the pigment to each visible light wavelength band is basically the same, and the bandgap of the pigment is 0.88 eV. The color of the pigment is black. The average grain size of spinels is only 26.795 nm, and the pigment has a superior thermal stability at 20-1 100 ℃. The ceramic has a good color performance when the pigment is used to prepare the ceramic. It is indicated that the prepared black ceramic pigment with the superior coloring property has a promising application potential.

, authors=Zhiqiao LI^{1, 2}, Xiang ZHANG^{1, 2}, Guojun MA¹, Dingli ZHENG¹, Mengke LIU², Qiang WANG², authorsList=Zhiqiao LI, Xiang ZHANG, Guojun MA, Dingli ZHENG, Mengke LIU, Qiang WANG, authorCompany=null, correspAuthors=Xiang ZHANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319986559353471138, articleId=1319986556471984288, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=不锈钢粉尘制备Fe-Cr-Ni-Mn系黑色陶瓷颜料, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

不锈钢粉尘中所富含的过渡金属元素，如Fe、Cr、Ni和Mn，可用于制备黑色陶瓷颜料，从而实现不锈钢粉尘的无害化、资源化利用，并可为无钴黑色陶瓷颜料的开发提供新途径。根据Fe-Cr-Ni-Mn系黑色颜料的呈色机理，在不锈钢粉尘中添加适量化学试剂Fe₂O₃、Cr₂O₃、MnO和NiO，调节上述组分在混合物料中摩尔比为6∶1∶1∶1。研究了不同工艺条件下所烧制黑色陶瓷颜料色度值的变化规律，并对颜料的呈色机理进行探讨。结果表明：烧制温度过高或保温时间过长都将导致含Cr尖晶石相分解，从而对颜料的呈色性能造成不利影响；颜料最佳烧制工艺为烧制温度1175 ℃、保温30 min、采用随炉冷却方式，所制备颜料的L*值、a*值和b*值分别为37.20、0.13与0.02，其所含主要物相为Fe₂O₃与复合尖晶石相；颜料对可见光各波段的吸光度基本一致，禁带宽度为0.88 eV，呈纯正黑色，同时颜料颗粒细小、粒径分布均匀、分散性好，尖晶石相平均晶粒尺寸为26.795 nm，且颜料在20~1100 ℃范围内显示出优异的热稳定性；将颜料应用于制备的陶瓷呈色效果良好，上述结果表明，所制备黑色陶瓷颜料具备优异的着色能力和应用潜力。

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LI Zhiqiao(1997-), male, Master candidate. E-mail: Lzq@wust.edu.cn

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LI Zhiqiao(1997-), male, Master candidate. E-mail: Lzq@wust.edu.cn

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