Article(id=1322943226491056493, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210667, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1628438400000, receivedDateStr=2021-08-09, revisedDate=1631030400000, revisedDateStr=2021-09-08, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343844291, onlineDateStr=2026-10-30, pubDate=1639929600000, pubDateStr=2021-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343844291, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343844291, creator=13701087609, updateTime=1793343844291, updator=13701087609, issue=Issue{id=1322943149844345666, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='12', pageStart='2549', pageEnd='2816', issueExtLink='null', onlineDate='null', pubDate='1639929600000', pubDateStr='2021-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343826018, creator='13701087609', updateTime=1793345974749, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322952162350859029, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322952162350859030, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2629, endPage=2635, ext={EN=ArticleExt(id=1322943228370104686, articleId=1322943226491056493, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Ablation Resistance of C/SiC Composites Prepared by Hot-pressed Sintering Process, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

C/SiC composites were prepared by the hot-pressed sintering process with SiC powder, carbon fiber and phenolic resin as raw materials. The effects of sintering pressure, sintering temperature and carbon fiber content on the ablation resistance of C/SiC composites were investigated via a designed orthogonal experiment. The phase composition, microstructure and ablation resistance of the samples were characterized by X-ray diffraction, scanning electron microscopy and oxygen-acetylene ablative method. The results show that the dominant factor affecting the ablation resistance of C/SiC composites is sintering temperature, while the minor factor is carbon fiber content. Increasing the sintering temperature and hot pressing pressure can be beneficial to the densification of the sample. However, the excessive sintering temperature and sintering pressure can promote the diffusion of Si element into carbon fiber that does not favor the ablative performance. In addition, the introduction of excessive carbon fiber is not conductive to the densification of the sample, thus leading to the ablation resistance reduction. With the sintering temperature of 2 050℃, the hot pressing pressure of 20 MPa and the volume fraction of carbon fiber of 25%, the obtained samples exhibit the superior ablation resistance with a mass ablation rate of 2.0 mg/s.

, authors=Hongxiang HUANG1, Feng WANG2, Zhiyong HE2, Xiaobo WANG2, authorsList=Hongxiang HUANG, Feng WANG, Zhiyong HE, Xiaobo WANG, authorCompany=null, correspAuthors=Zhiyong HE, authorNote=

HUANG Hongxiang (1996-), male, Master candidate. E-mail:

, correspAuthorsNote=
HE Zhiyong (1970-), male, Professorate Senior Engineer. E-mail:
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以SiC粉、碳纤维和酚醛树脂为主要原料,采用热压工艺制备了C/SiC复合材料。采用正交试验法研究了碳纤维含量、烧结温度和烧结压力对C/SiC复合材料抗烧蚀性能的影响。采用X射线衍射仪、电子扫描显微镜及氧-乙炔烧蚀法对样品物相组成、显微结构及抗烧蚀性能进行表征。结果表明:烧结温度对C/SiC复合材料的抗烧蚀性能影响最大,其次为碳纤维含量。烧结温度与热压压力的提高有助于样品的致密化烧结,但过高的烧结温度与热压压力会促进Si元素向碳纤维扩散,对抗烧蚀性能不利。过多碳纤维的引入不利于样品致密化,会导致抗烧蚀性能降低。当烧结温度为2 050℃,热压压力为20 MPa、碳纤维含量为25%(体积分数)时,C/SiC复合材料抗烧蚀性能最好,质量烧蚀率为2.0 mg/s。

, authors=黄竑翔1, 王峰2, 贺智勇2, 王晓波2, authorsList=黄竑翔, 王峰, 贺智勇, 王晓波, authorCompany=null, correspAuthors=贺智勇, authorNote=

黄竑翔(1996—),男,硕士研究生。

, correspAuthorsNote=
贺智勇(1970—),男,正高级工程师。
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黄竑翔(1996—),男,硕士研究生。

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黄竑翔(1996—),男,硕士研究生。

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热压烧结工艺制备C/SiC复合材料的抗烧蚀性能
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黄竑翔 1 , 王峰 2 , 贺智勇 2 , 王晓波 2
硅酸盐学报 | 研究论文 2021,49(12): 2629-2635
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硅酸盐学报 |研究论文 2021 , 49 (12) : 2629 -2635
热压烧结工艺制备C/SiC复合材料的抗烧蚀性能
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黄竑翔1 , 王峰2, 贺智勇2 , 王晓波2
作者信息
  • 1.钢铁研究总院,北京 100081
  • 2.中国钢研科技集团有限公司,北京 100081
通讯作者:
贺智勇(1970—),男,正高级工程师。
作者简介:

黄竑翔(1996—),男,硕士研究生。

Ablation Resistance of C/SiC Composites Prepared by Hot-pressed Sintering Process
Hongxiang HUANG1 , Feng WANG2, Zhiyong HE2 , Xiaobo WANG2
Affiliations
  • 1.Central Iron&Steel Research Institute, Beijing 100081, China
  • 2.China Iron & Steel Research Institute Group, Beijing 100081, China
  • Corresponding Author:
    HE Zhiyong (1970-), male, Professorate Senior Engineer. E-mail:

    HUANG Hongxiang (1996-), male, Master candidate. E-mail:

出版时间: 2021-12-20 doi: 10.14062/j.issn.0454-5648.20210667
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以SiC粉、碳纤维和酚醛树脂为主要原料,采用热压工艺制备了C/SiC复合材料。采用正交试验法研究了碳纤维含量、烧结温度和烧结压力对C/SiC复合材料抗烧蚀性能的影响。采用X射线衍射仪、电子扫描显微镜及氧-乙炔烧蚀法对样品物相组成、显微结构及抗烧蚀性能进行表征。结果表明:烧结温度对C/SiC复合材料的抗烧蚀性能影响最大,其次为碳纤维含量。烧结温度与热压压力的提高有助于样品的致密化烧结,但过高的烧结温度与热压压力会促进Si元素向碳纤维扩散,对抗烧蚀性能不利。过多碳纤维的引入不利于样品致密化,会导致抗烧蚀性能降低。当烧结温度为2 050℃,热压压力为20 MPa、碳纤维含量为25%(体积分数)时,C/SiC复合材料抗烧蚀性能最好,质量烧蚀率为2.0 mg/s。

碳/碳化硅复合材料  /  烧结温度  /  碳纤维含量  /  热压压力  /  抗烧蚀

C/SiC composites were prepared by the hot-pressed sintering process with SiC powder, carbon fiber and phenolic resin as raw materials. The effects of sintering pressure, sintering temperature and carbon fiber content on the ablation resistance of C/SiC composites were investigated via a designed orthogonal experiment. The phase composition, microstructure and ablation resistance of the samples were characterized by X-ray diffraction, scanning electron microscopy and oxygen-acetylene ablative method. The results show that the dominant factor affecting the ablation resistance of C/SiC composites is sintering temperature, while the minor factor is carbon fiber content. Increasing the sintering temperature and hot pressing pressure can be beneficial to the densification of the sample. However, the excessive sintering temperature and sintering pressure can promote the diffusion of Si element into carbon fiber that does not favor the ablative performance. In addition, the introduction of excessive carbon fiber is not conductive to the densification of the sample, thus leading to the ablation resistance reduction. With the sintering temperature of 2 050℃, the hot pressing pressure of 20 MPa and the volume fraction of carbon fiber of 25%, the obtained samples exhibit the superior ablation resistance with a mass ablation rate of 2.0 mg/s.

carbon/silicon carbide composites  /  sintering temperature  /  carbon fiber content  /  hot-pressing pressure  /  ablation resistance
黄竑翔, 王峰, 贺智勇, 王晓波. 热压烧结工艺制备C/SiC复合材料的抗烧蚀性能. 硅酸盐学报, 2021 , 49 (12) : 2629 -2635 . DOI: 10.14062/j.issn.0454-5648.20210667
Hongxiang HUANG, Feng WANG, Zhiyong HE, Xiaobo WANG. Ablation Resistance of C/SiC Composites Prepared by Hot-pressed Sintering Process[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (12) : 2629 -2635 . DOI: 10.14062/j.issn.0454-5648.20210667

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2021年第49卷第12期
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doi: 10.14062/j.issn.0454-5648.20210667
  • 接收时间:2021-08-09
  • 首发时间:2026-10-30
  • 出版时间:2021-12-20
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  • 收稿日期:2021-08-09
  • 修回日期:2021-09-08
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    1.钢铁研究总院,北京 100081
    2.中国钢研科技集团有限公司,北京 100081

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贺智勇(1970—),男,正高级工程师。
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2种不同金属材料的力学参数
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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