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Lithium cobalt oxide is a leading cathode material for 3C electronic products because of its high bulk energy density, excellent rate capacity and good cycle performance. The existing gram capacity of lithium cobalt oxide material in practical application is approximately 65% of the theoretical capacity, and this material has a potential for further development. In this paper, a lithium ion cobalt oxide cathode material was coated with lithium ion conductor material LiAlSiO₄ by a sol-gel method. The effects of LiAlSiO₄ and heat treatment temperature on the structure, morphology and electrochemical properties of the material were investigated. The results show that during the heat treatment, Al³⁺ enters the LiCoO₂ lattice to form a solid solution LiCo_1-xAl_xO₂, and an inert coating layer is formed on the surface of the lithium cobalt oxide particles LiAlSiO₄ coating, effectively improving the cycle and rate performance of the lithium cobalt oxide material at a high voltage. The optimum overall performance of the lithium cobalt oxide material coated with LiAlSiO₄ can be obtained at a heat treatment temperature of 600 ℃. In a voltage range of 2.75-4.55 V, the specific discharge capacity at room temperature at 0.5 C rate is 209.3 mA·h/g, and the discharge specific capacity after 50 cycles is 201.6 mA·h/g (at a capacity retention rate of 96.3%), and the specific capacity is 160.0 mA·h/g at 8 C.

, authors=Bin SHEN¹, Xing XU², Wanmin LIU¹, Mulan QIN¹, Weigang WANG¹, authorsList=Bin SHEN, Xing XU, Wanmin LIU, Mulan QIN, Weigang WANG, authorCompany=null, correspAuthors=Wanmin LIU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319986872869310610, articleId=1319986872395354256, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=LiAlSiO₄改性高电压LiCoO₂正极材料的电化学性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

钴酸锂因其高体积能量密度、优异的倍率容量和良好的循环性能，是3C类电子产品的主导正极材料，且目前实际应用的钴酸锂材料克容量约为理论容量的65%，还具有进一步开发的潜力。采用溶胶-凝胶法对正极材料LiCoO₂进行锂离子导体材料LiAlSiO₄包覆，研究了LiAlSiO₄及热处理温度对材料结构、形貌和电化学性能的影响。结果表明：热处理过程中Al³⁺可进入LiCoO₂晶格，形成固溶体LiCo_1-xAl_xO₂；LiAlSiO₄在钴酸锂颗粒表面形成惰性的包覆层，有效地改善了钴酸锂材料在高电压下的循环和倍率性能。当热处理温度为600 ℃时，LiAlSiO₄包覆的钴酸锂材料综合性能达到最优。该样品在2.75~4.55 V的电压范围内，0.5 C倍率下室温放电比容量为209.3 mA·h/g，50次循环后的放电比容量为201.6 mA·h/g（容量保留率96.3%），且在8 C倍率下依然能释放出160.0 mA·h/g的比容量。

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SHEN Bin (1986-), male, Ph.D.. E-mail: shenbin1986@126.com

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申斌（1986—），男，博士。

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申斌（1986—），男，博士。

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