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Article(id=1319986920353026505, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986871980118160, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210554, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1625068800000, receivedDateStr=2021-07-01, revisedDate=1631635200000, revisedDateStr=2021-09-15, acceptedDate=null, acceptedDateStr=null, onlineDate=1792639005983, onlineDateStr=2026-10-22, pubDate=1652976000000, pubDateStr=2022-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792639005983, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792639005983, creator=13701087609, updateTime=1792639005983, updator=13701087609, issue=Issue{id=1319986871980118160, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='5', pageStart='1201', pageEnd='1454', issueExtLink='null', onlineDate='null', pubDate='1652976000000', pubDateStr='2022-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792638994450, creator='13701087609', updateTime=1792639285419, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319988092451275233, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986871980118160, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319988092451275234, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319986871980118160, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1283, endPage=1291, ext={EN=ArticleExt(id=1319986920579518922, articleId=1319986920353026505, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Titanium Dioxide on Crystallization Behavior and Properties of MgO-Al2O3-SiO2 Glass-Ceramics, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Cordierite glass-ceramics exhibit low dielectric constant, dielectric loss and thermal expansion. The stoichiometric cordierite MgO-Al2O3-SiO2 (MAS) glass is due to the surface crystallization. In this paper, MAS glass-ceramics with various contents of TiO2 as a nucleation agent were prepared by a melting method and subsequent heat treatment. The effect of TiO2 content on the crystallization behavior and properties was investigated. The results show that the glass transition temperature and the first crystallization peak temperature decrease with the increase of TiO2 content, indicating that TiO2 can effectively promote the crystallization. TiO2 enters into the glass network structure, and facilitates the formation of μ-cordierite and magnesium aluminum titanate crystalline phases in the glass, and then form α-cordierite at a higher temperature. The crystallization mechanism of glass with more than 5% (in molar fraction) TiO2 becomes the bulk crystallization. As TiO2 content increases to 10%, the glass-ceramics heat-treated at 800 ℃ for 10 h and 1 000 ℃ for 5 h have a high density of 2.95 g/cm3, a hardness of 9.67 GPa, and a thermal conductivity of 2.13 W/(m·K). At 8.2-12.4 GHz, its dielectric constant is 6.3-6.5 and the dielectric loss fluctuates from 10-2 to 10-3. At 1 MHz, the dielectric constant is 10.8 and the dielectric loss is 0.024 4.

, authors=Wei YU1, Xinhui LIANG2, Shuzhi LI2, Wenkai GAO1, Zhanmeng ZHANG1, Bo ZHONG2, Jing WANG1, Jianjun HAN1, authorsList=Wei YU, Xinhui LIANG, Shuzhi LI, Wenkai GAO, Zhanmeng ZHANG, Bo ZHONG, Jing WANG, Jianjun HAN, authorCompany=null, correspAuthors=Jing WANG, authorNote=

YU Wei (1995-), male, Master candidate. E-mail:

, correspAuthorsNote=
WANG Jing (1988-), female, Ph.D., Associate Professor. E-mail:
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堇青石微晶玻璃具有低介电常数、低介电损耗、低热膨胀等优点，化学计量堇青石MgO-Al2O3-SiO2（MAS）玻璃组成易表面析晶。采用熔融-整体析晶法制备了MAS微晶玻璃，研究了TiO2添加量对MAS微晶玻璃析晶行为和性能的影响。随着TiO2添加量的增加，玻璃化转变温度和第1析晶峰温度降低，说明TiO2能够有效促进析晶。TiO2进入玻璃网络结构中，促进玻璃中先形成μ-堇青石和钛酸镁铝相，在较高温度下转变为α-堇青石。当x（TiO2）>5%（摩尔分数）时玻璃结晶机制为体析晶。当TiO2含量增加到10%时，经800 ℃保温10 h+1 000 ℃保温5 h热处理的微晶玻璃具有高密度2.95 g/cm3，高硬度9.67 GPa，高热导率2.13 W/（m·K）。在频率为8.2~12.4 GHz，其介电常数为6.3~6.5，介电损耗在10-2~10-3内波动，在频率为1 MHz，介电常数为10.8，介电损耗为0.024 4。

, authors=余炜1, 梁新辉2, 李书志2, 高文凯1, 张占蒙1, 钟波2, 王静1, 韩建军1, authorsList=余炜, 梁新辉, 李书志, 高文凯, 张占蒙, 钟波, 王静, 韩建军, authorCompany=null, correspAuthors=王静, authorNote=

余炜（1995—），男，硕士。

, correspAuthorsNote=
王静（1988—），女，博士，副研究员。
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YU Wei (1995-), male, Master candidate. E-mail:

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余炜（1995—），男，硕士。

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余炜（1995—），男，硕士。

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二氧化钛对镁铝硅微晶玻璃析晶行为与性能的影响
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余炜 1 , 梁新辉 2 , 李书志 2 , 高文凯 1 , 张占蒙 1 , 钟波 2 , 王静 1 , 韩建军 1
硅酸盐学报 | 研究论文 2022,50(5): 1283-1291
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硅酸盐学报 |研究论文 2022 , 50 (5) : 1283 -1291
二氧化钛对镁铝硅微晶玻璃析晶行为与性能的影响
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YU Wei (1995-), male, Master candidate. E-mail:

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余炜（1995—），男，硕士。

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余炜1 , 梁新辉2, 李书志2, 高文凯1, 张占蒙1, 钟波2, 王静1 , 韩建军1
作者信息
  • 1．武汉理工大学，硅酸盐建筑材料国家重点实验室，武汉 4300702
  • 2．咸宁南玻光电玻璃有限公司，湖北 咸宁 437100
通讯作者:
王静（1988—），女，博士，副研究员。
作者简介:

余炜（1995—），男，硕士。

Effect of Titanium Dioxide on Crystallization Behavior and Properties of MgO-Al2O3-SiO2 Glass-Ceramics
Wei YU1 , Xinhui LIANG2, Shuzhi LI2, Wenkai GAO1, Zhanmeng ZHANG1, Bo ZHONG2, Jing WANG1 , Jianjun HAN1
Affiliations
  • 1.State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan 430070, China
  • 2.Xianning SG photoelectric glass Co. Ltd., Xianning 437100, Hubei, China
    • Corresponding Author:
    WANG Jing (1988-), female, Ph.D., Associate Professor. E-mail:

    YU Wei (1995-), male, Master candidate. E-mail:

出版时间: 2022-05-20 doi: 10.14062/j.issn.0454-5648.20210554
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堇青石微晶玻璃具有低介电常数、低介电损耗、低热膨胀等优点，化学计量堇青石MgO-Al2O3-SiO2（MAS）玻璃组成易表面析晶。采用熔融-整体析晶法制备了MAS微晶玻璃，研究了TiO2添加量对MAS微晶玻璃析晶行为和性能的影响。随着TiO2添加量的增加，玻璃化转变温度和第1析晶峰温度降低，说明TiO2能够有效促进析晶。TiO2进入玻璃网络结构中，促进玻璃中先形成μ-堇青石和钛酸镁铝相，在较高温度下转变为α-堇青石。当x（TiO2）>5%（摩尔分数）时玻璃结晶机制为体析晶。当TiO2含量增加到10%时，经800 ℃保温10 h+1 000 ℃保温5 h热处理的微晶玻璃具有高密度2.95 g/cm3，高硬度9.67 GPa，高热导率2.13 W/（m·K）。在频率为8.2~12.4 GHz，其介电常数为6.3~6.5，介电损耗在10-2~10-3内波动，在频率为1 MHz，介电常数为10.8，介电损耗为0.024 4。

微晶玻璃  /  堇青石  /  表面析晶  /  介电性能  /  二氧化钛

Cordierite glass-ceramics exhibit low dielectric constant, dielectric loss and thermal expansion. The stoichiometric cordierite MgO-Al2O3-SiO2 (MAS) glass is due to the surface crystallization. In this paper, MAS glass-ceramics with various contents of TiO2 as a nucleation agent were prepared by a melting method and subsequent heat treatment. The effect of TiO2 content on the crystallization behavior and properties was investigated. The results show that the glass transition temperature and the first crystallization peak temperature decrease with the increase of TiO2 content, indicating that TiO2 can effectively promote the crystallization. TiO2 enters into the glass network structure, and facilitates the formation of μ-cordierite and magnesium aluminum titanate crystalline phases in the glass, and then form α-cordierite at a higher temperature. The crystallization mechanism of glass with more than 5% (in molar fraction) TiO2 becomes the bulk crystallization. As TiO2 content increases to 10%, the glass-ceramics heat-treated at 800 ℃ for 10 h and 1 000 ℃ for 5 h have a high density of 2.95 g/cm3, a hardness of 9.67 GPa, and a thermal conductivity of 2.13 W/(m·K). At 8.2-12.4 GHz, its dielectric constant is 6.3-6.5 and the dielectric loss fluctuates from 10-2 to 10-3. At 1 MHz, the dielectric constant is 10.8 and the dielectric loss is 0.024 4.

glass-ceramics  /  cordierite  /  surface crystallization  /  dielectric properties  /  titanium dioxide
余炜, 梁新辉, 李书志, 高文凯, 张占蒙, 钟波, 王静, 韩建军. 二氧化钛对镁铝硅微晶玻璃析晶行为与性能的影响. 硅酸盐学报, 2022 , 50 (5) : 1283 -1291 . DOI: 10.14062/j.issn.0454-5648.20210554
Wei YU, Xinhui LIANG, Shuzhi LI, Wenkai GAO, Zhanmeng ZHANG, Bo ZHONG, Jing WANG, Jianjun HAN. Effect of Titanium Dioxide on Crystallization Behavior and Properties of MgO-Al2O3-SiO2 Glass-Ceramics[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (5) : 1283 -1291 . DOI: 10.14062/j.issn.0454-5648.20210554
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  • 国家自然科学基金(52072278)
  • 中央高校基础研究经费项目(WUT：2021ZVA124)
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doi: 10.14062/j.issn.0454-5648.20210554
  • 接收时间：2021-07-01
  • 首发时间：2026-10-22
  • 出版时间：2022-05-20
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  • 收稿日期：2021-07-01
  • 修回日期：2021-09-15
基金
国家自然科学基金(52072278)
中央高校基础研究经费项目(WUT：2021ZVA124)
作者信息
    1．武汉理工大学，硅酸盐建筑材料国家重点实验室，武汉 4300702
    2．咸宁南玻光电玻璃有限公司，湖北 咸宁 437100

通讯作者:

王静（1988—），女，博士，副研究员。
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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