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Article(id=1322943941313700555, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210284, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1618588800000, receivedDateStr=2021-04-17, revisedDate=1619798400000, revisedDateStr=2021-05-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1793344014719, onlineDateStr=2026-10-30, pubDate=1639929600000, pubDateStr=2021-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793344014719, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793344014719, creator=13701087609, updateTime=1793344014719, updator=13701087609, issue=Issue{id=1322943149844345666, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='12', pageStart='2549', pageEnd='2816', issueExtLink='null', onlineDate='null', pubDate='1639929600000', pubDateStr='2021-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343826018, creator='13701087609', updateTime=1793345974749, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322952162350859029, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322952162350859030, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2776, endPage=2782, ext={EN=ArticleExt(id=1322943941582136012, articleId=1322943941313700555, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Stability of Strontium Zirconate Crucible for Induction Melting of Ti2Ni Alloys, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

A strontium zirconate oxide refractory was prepared by a solid-state reaction method at a mole ratio n(SrO): n(ZrO2) of 2∶1 and 1 400℃, and Ti2Ni alloys were melted in a crucible at 1 750℃. The phase composition and microstructure of the refractory as well as the key features of Ti2Ni alloy melt interacted with the refractory crucible were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and optical microscopy (OM). The results reveal that the crucible refractory is consisted with the phases of Sr2ZrO4, Sr3Zr2O7 and SrO, respectively. The thermodynamically stable phase Sr2ZrO4 is unable to obtain separately due to the limitation of the reaction between SrCO3 and ZrO2, causing the residues of Sr3Zr2O7 and SrO. The thickness of interaction layer for the strontium zirconate oxide and barium zirconate crucible are 1 250 μm and 2 120 μm, respectively. The oxygen concentrations of the alloy after melting in strontium zirconate oxide and barium zirconate crucible are 0.332% and 0.566% (in mass fraction), respectively. It is indicated that the strontium zirconate oxide refractory exhibits a superior stability, compared to the barium zirconate refractory.

, authors=Guangyao CHEN1, 2, Feihai YU1, Xiao HOU1, Yuchen YANG1, Yubin XIAO1, Yin ZHANG1, Xingli ZOU1, Xinmei HOU3, Xionggang LU1, 2, Chonghe LI1, 2, authorsList=Guangyao CHEN, Feihai YU, Xiao HOU, Yuchen YANG, Yubin XIAO, Yin ZHANG, Xingli ZOU, Xinmei HOU, Xionggang LU, Chonghe LI, authorCompany=null, correspAuthors=Xinmei HOU, Chonghe LI, authorNote=

CHEN Guangyao(1987-), Male, Ph.D., Lecturer. E-mail:

, correspAuthorsNote=
LI Chonghe(1962-), Male, Ph.D., Professor. E-mail:
HOU Xinmei(1979-), Female, Ph.D., Professor.
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以SrCO3和ZrO2为原料、二者摩尔比为2∶1，在1 400℃通过高温固相合成法制备了锆酸锶质氧化物耐火材料，并在1 750℃烧成制备坩埚，将其用于富钛含量Ti2Ni合金的感应熔炼，并与锆酸钡坩埚在合金熔炼的稳定性表现进行了对比研究。通过X射线衍射仪，扫描电子显微镜和光学显微镜，分析研究了锆酸锶质氧化物耐火材料的相组成及微结构，耐火材料与钛合金熔体的界面反应层及熔体受耐火材料的污染程度。结果表明：锆酸锶质氧化物耐火材料主要由Sr3Zr2O7、Sr2ZrO4和SrO三相共存，动力学反应时间不足是导致Sr2ZrO4单相无法生成的主要原因。锆酸锶质氧化物和锆酸钡坩埚熔炼Ti2Ni合金后的坩埚受侵蚀层分别为1 250 μm和2 120 μm，而合金中氧含量平均值分别为0.332%（质量分数）和0.566%。说明锆酸锶质氧化物耐火材料对Ti2Ni合金熔体稳定性优于锆酸钡耐火材料。

, authors=陈光耀1, 2, 余飞海1, 侯笑1, 杨宇辰1, 肖玉彬1, 张胤1, 邹星礼1, 侯新梅3, 鲁雄刚1, 2, 李重河1, 2, *, authorsList=陈光耀, 余飞海, 侯笑, 杨宇辰, 肖玉彬, 张胤, 邹星礼, 侯新梅, 鲁雄刚, 李重河, authorCompany=null, correspAuthors=侯新梅, 李重河, authorNote=

陈光耀（1987—），男，博士，讲师。

, correspAuthorsNote=
李重河（1962—），男，博士，教授。
侯新梅（1979—），女，博士，教授。
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2.Shanghai Special Casting Engineering Technology Research Center, Shanghai 201605, China, bio={"content":"

CHEN Guangyao(1987-), Male, Ph.D., Lecturer. E-mail:

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CHEN Guangyao(1987-), Male, Ph.D., Lecturer. E-mail:

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Ti2Ni合金感应熔炼用锆酸锶质坩埚稳定性评价
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陈光耀 1, 2 , 余飞海 1 , 侯笑 1 , 杨宇辰 1 , 肖玉彬 1 , 张胤 1 , 邹星礼 1 , 侯新梅 3 , 鲁雄刚 1, 2 , 李重河 1, 2, *
硅酸盐学报 | 研究论文 2021,49(12): 2776-2782
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硅酸盐学报 |研究论文 2021 , 49 (12) : 2776 -2782
Ti2Ni合金感应熔炼用锆酸锶质坩埚稳定性评价
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陈光耀1, 2 , 余飞海1, 侯笑1, 杨宇辰1, 肖玉彬1, 张胤1, 邹星礼1, 侯新梅3 , 鲁雄刚1, 2, 李重河1, 2, *
作者信息
  • 1．上海大学材料科学与工程学院，省部共建高品质特殊钢冶金与制备国家重点实验室，上海市钢铁冶金新技术开发应用重点实验室，上海 200072
  • 2．上海市特种铸造工程技术研究中心，上海 201605
  • 3．北京科技大学钢铁共性技术协同创新中心，北京 100083
通讯作者:
李重河（1962—），男，博士，教授。
侯新梅（1979—），女，博士，教授。
作者简介:

陈光耀（1987—），男，博士，讲师。

Stability of Strontium Zirconate Crucible for Induction Melting of Ti2Ni Alloys
Guangyao CHEN1, 2 , Feihai YU1, Xiao HOU1, Yuchen YANG1, Yubin XIAO1, Yin ZHANG1, Xingli ZOU1, Xinmei HOU3 , Xionggang LU1, 2, Chonghe LI1, 2
Affiliations
  • 1.State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy, School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
  • 2.Shanghai Special Casting Engineering Technology Research Center, Shanghai 201605, China
  • 3.Collaborative Innovation Center of Steel Technology, University of Science and Technology Beijing, Beijing 100083, China
    • Corresponding Author:
    LI Chonghe(1962-), Male, Ph.D., Professor. E-mail:
    HOU Xinmei(1979-), Female, Ph.D., Professor.

    CHEN Guangyao(1987-), Male, Ph.D., Lecturer. E-mail:

出版时间: 2021-12-20 doi: 10.14062/j.issn.0454-5648.20210284
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以SrCO3和ZrO2为原料、二者摩尔比为2∶1，在1 400℃通过高温固相合成法制备了锆酸锶质氧化物耐火材料，并在1 750℃烧成制备坩埚，将其用于富钛含量Ti2Ni合金的感应熔炼，并与锆酸钡坩埚在合金熔炼的稳定性表现进行了对比研究。通过X射线衍射仪，扫描电子显微镜和光学显微镜，分析研究了锆酸锶质氧化物耐火材料的相组成及微结构，耐火材料与钛合金熔体的界面反应层及熔体受耐火材料的污染程度。结果表明：锆酸锶质氧化物耐火材料主要由Sr3Zr2O7、Sr2ZrO4和SrO三相共存，动力学反应时间不足是导致Sr2ZrO4单相无法生成的主要原因。锆酸锶质氧化物和锆酸钡坩埚熔炼Ti2Ni合金后的坩埚受侵蚀层分别为1 250 μm和2 120 μm，而合金中氧含量平均值分别为0.332%（质量分数）和0.566%。说明锆酸锶质氧化物耐火材料对Ti2Ni合金熔体稳定性优于锆酸钡耐火材料。

钛合金  /  锆酸锶  /  耐火材料  /  感应熔炼  /  界面反应

A strontium zirconate oxide refractory was prepared by a solid-state reaction method at a mole ratio n(SrO): n(ZrO2) of 2∶1 and 1 400℃, and Ti2Ni alloys were melted in a crucible at 1 750℃. The phase composition and microstructure of the refractory as well as the key features of Ti2Ni alloy melt interacted with the refractory crucible were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and optical microscopy (OM). The results reveal that the crucible refractory is consisted with the phases of Sr2ZrO4, Sr3Zr2O7 and SrO, respectively. The thermodynamically stable phase Sr2ZrO4 is unable to obtain separately due to the limitation of the reaction between SrCO3 and ZrO2, causing the residues of Sr3Zr2O7 and SrO. The thickness of interaction layer for the strontium zirconate oxide and barium zirconate crucible are 1 250 μm and 2 120 μm, respectively. The oxygen concentrations of the alloy after melting in strontium zirconate oxide and barium zirconate crucible are 0.332% and 0.566% (in mass fraction), respectively. It is indicated that the strontium zirconate oxide refractory exhibits a superior stability, compared to the barium zirconate refractory.

titanium alloys  /  zirconate strontium  /  refractory  /  induction melting  /  interaction
陈光耀, 余飞海, 侯笑, 杨宇辰, 肖玉彬, 张胤, 邹星礼, 侯新梅, 鲁雄刚, 李重河. Ti2Ni合金感应熔炼用锆酸锶质坩埚稳定性评价. 硅酸盐学报, 2021 , 49 (12) : 2776 -2782 . DOI: 10.14062/j.issn.0454-5648.20210284
Guangyao CHEN, Feihai YU, Xiao HOU, Yuchen YANG, Yubin XIAO, Yin ZHANG, Xingli ZOU, Xinmei HOU, Xionggang LU, Chonghe LI. Stability of Strontium Zirconate Crucible for Induction Melting of Ti2Ni Alloys[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (12) : 2776 -2782 . DOI: 10.14062/j.issn.0454-5648.20210284
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  • 国家自然科学基金面上项目(52022054; 51974181; 51974021)
  • 国家自然科学基金杰出青年基金(No.52025041)
  • 上海高校特聘教授（东方学者）岗位计划(TP2019041)
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2021年第49卷第12期
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doi: 10.14062/j.issn.0454-5648.20210284
  • 接收时间：2021-04-17
  • 首发时间：2026-10-30
  • 出版时间：2021-12-20
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  • 收稿日期：2021-04-17
  • 修回日期：2021-05-01
基金
国家自然科学基金面上项目(52022054; 51974181; 51974021)
国家自然科学基金杰出青年基金(No.52025041)
上海高校特聘教授（东方学者）岗位计划(TP2019041)
作者信息
    1．上海大学材料科学与工程学院，省部共建高品质特殊钢冶金与制备国家重点实验室，上海市钢铁冶金新技术开发应用重点实验室，上海 200072
    2．上海市特种铸造工程技术研究中心，上海 201605
    3．北京科技大学钢铁共性技术协同创新中心，北京 100083

通讯作者:

李重河（1962—），男，博士，教授。
侯新梅（1979—），女，博士，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20210284
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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