Article(id=1322943172023825401, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210193, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1616515200000, receivedDateStr=2021-03-24, revisedDate=1618848000000, revisedDateStr=2021-04-20, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343831306, onlineDateStr=2026-10-30, pubDate=1639929600000, pubDateStr=2021-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343831306, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343831306, creator=13701087609, updateTime=1793343831306, updator=13701087609, issue=Issue{id=1322943149844345666, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='12', pageStart='2549', pageEnd='2816', issueExtLink='null', onlineDate='null', pubDate='1639929600000', pubDateStr='2021-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343826018, creator='13701087609', updateTime=1793345974749, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322952162350859029, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322952162350859030, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2767, endPage=2775, ext={EN=ArticleExt(id=1322943172233540602, articleId=1322943172023825401, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=High-temperature Nitriding Mechanism of Al₄O₄C, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

The phase transformation, structure evolution and reaction mechanism of Al₄O₄C in high-temperature nitrogen were investigated. The experimental results indicate that Al₄O₄C reacts with nitrogen at > 7 00℃, and the nitridation reaction is composed of several cyclic processes, i.e., surface reaction, internal diffusion and mass transfer reaction. In the initial stage, nitridation reaction occurs on the surface to form a composite reaction layer of AlN, Al₂O₃, and C, which inhibits the diffusion of nitrogen. The nitridation reaction rate increases and the volume expansion effect associated with the formation of a large amount of AlN causes Al₄O₄C reaction layer to crack when the temperature increases. The loose and porous surface structure from the staggered growth of Al₂O₃ and AlN as gas diffusion channels can accelerate nitrogen diffusion and reaction. When the nitridation temperature is 1 600℃, the intermediate products of Al₂O₃, C, and N₂ undergo a carbon-thermal reduction and nitridation reaction, accompanied with massive gas phase generation. The more sufficient the AlN particles develop, the more complete the crystal grain morphology will be.

, authors=Guangchao XING, Chengji DENG, Keren CHENG, Jun DING, Hongxi ZHU, Jinghui DI, Chao YU, authorsList=Guangchao XING, Chengji DENG, Keren CHENG, Jun DING, Hongxi ZHU, Jinghui DI, Chao YU, authorCompany=null, correspAuthors=Chao YU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943172493587451, articleId=1322943172023825401, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Al₄O₄C材料的高温氮化机理, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

研究了Al₄O₄C材料在高温氮气条件下的物相转化、结构演变与反应机理。结果表明：Al₄O₄C在高于700℃氮气气氛条件下开始发生反应，其氮化反应是由表面反应和内部扩散传质反应的若干个循环过程组成的。在反应初始阶段，Al₄O₄C材料表面发生氮化反应并形成AlN、Al₂O₃、C复合反应层，阻碍氮气的扩散。随着热处理温度的升高，氮化反应速率加快，大量AlN形成伴随的体积膨胀效应造成Al₄O₄C表面反应层破裂，AlN和Al₂O₃交错生长的疏松多孔表面结构作为气相扩散通道，促进氮气扩散与反应。当氮化温度为1 600℃时，中间产物Al₂O₃、C和N₂进一步发生碳热还原氮化反应，并伴随大量气相生成，AlN颗粒发育更为完全，晶粒形貌更完整。

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XING Guangchao(1994-), male, Doctorial candidate. E-mail: guangchaoxing@hotmail.com

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邢广超（1994—），男，博士研究生。

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邢广超（1994—），男，博士研究生。

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