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Article(id=1319987060367274793, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319987055371858691, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210182, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1615737600000, receivedDateStr=2021-03-15, revisedDate=1624550400000, revisedDateStr=2021-06-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1792639039365, onlineDateStr=2026-10-22, pubDate=1645286400000, pubDateStr=2022-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792639039365, onlineIssueDateStr=2026-10-22, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792639039365, creator=13701087609, updateTime=1792639039365, updator=13701087609, issue=Issue{id=1319987055371858691, tenantId=1146029695717560320, journalId=1263187385517883426, year='2022', volume='50', issue='2', pageStart='277', pageEnd='554', issueExtLink='null', onlineDate='null', pubDate='1645286400000', pubDateStr='2022-02-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1792639038174, creator='13701087609', updateTime=1792639254308, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319987961958089069, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319987055371858691, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319987961958089070, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1319987055371858691, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=372, endPage=377, ext={EN=ArticleExt(id=1319987060581184298, articleId=1319987060367274793, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Zirconia on Mechanical Properties of Chemically Strengthened Lithium Aluminosilicate Glasses, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Lithium-aluminosilicate glasses with different zirconia (ZrO2) concentrations were prepared by a melting-quenching method. Glass slices were treated using a two-step chemical strengthening method below glass transition temperature (Tg). The effect of ZrO2 addition on the glass stability, hardness and chemical strengthening performance was investigated. The results show that the Tg increases with the increase of ZrO2 concentration in the range of 0-5% (in mole fraction). The absence of crystallization peaks indicates these glasses are rather stable. An appropriate addition of ZrO2 can promote the Li+-Na+ ions exchange and increase the layer depth. The surface compression stress (σc) increases with the increase of the ZrO2 concentration and reaches a maximum value of 1 055.6 MPa at 4% ZrO2 concentration. The center tension firstly increases and then decreases slightly with the increase of the ZrO2 concentration, indicating that these glass samples have a good shock resistance. The addition of ZrO2 has little effect on the hardness of glasses after chemical strengthening. Although the addition of ZrO2 decreases the crack resistance, these glasses still have a good crack resistance performance after chemical strengthening.

, authors=Jin HE1, Mingzhong WANG1, Zhihong CHEN1, Shuzhi LI1, Yinsheng XU2, Ping LU2, authorsList=Jin HE, Mingzhong WANG, Zhihong CHEN, Shuzhi LI, Yinsheng XU, Ping LU, authorCompany=null, correspAuthors=Ping LU, authorNote=

HE Jin (1972-), male, Master, Senior Engineer. E-mail:

, correspAuthorsNote=
LU Ping (1977-), male, Ph.D., Associate Professor. E-mail:
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采用熔融淬冷法制备了含不同摩尔分数ZrO2的锂铝硅酸盐玻璃，通过两步化学强化法对玻璃样片进行了化学强化，研究了ZrO2对玻璃的稳定性、硬度和化学强化效果的影响。结果表明：随着ZrO2的摩尔分数从0增加至5%，玻璃化转变温度随之升高，玻璃稳定无析晶现象。引入适量的ZrO2会促进Li+-Na+离子交换，提高应力层深度，表面压应力随着ZrO2浓度的增加而增加，并在摩尔分数为4%时达到最大值，为1 055.6 MPa。中心张应力随着ZrO2浓度的增加先增加后缓慢减小，表明该系列样品具有较好的抗冲击能力。ZrO2的浓度变化对强化后玻璃的硬度影响较小，在引入ZrO2后其抗裂性有所降低，但仍具有较好的抗裂能力。

, authors=何进1, 王明忠1, 陈志鸿1, 李书志1, 许银生2, 陆平2, authorsList=何进, 王明忠, 陈志鸿, 李书志, 许银生, 陆平, authorCompany=null, correspAuthors=陆平, authorNote=

何进（1972—），男，硕士，高级工程师。

, correspAuthorsNote=
陆平（1977—），男，博士，副研究员。
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HE Jin (1972-), male, Master, Senior Engineer. E-mail:

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何进（1972—），男，硕士，高级工程师。

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氧化锆对锂铝硅酸盐玻璃化学强化性能的影响
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何进 1 , 王明忠 1 , 陈志鸿 1 , 李书志 1 , 许银生 2 , 陆平 2
硅酸盐学报 | 研究论文 2022,50(2): 372-377
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硅酸盐学报 |研究论文 2022 , 50 (2) : 372 -377
氧化锆对锂铝硅酸盐玻璃化学强化性能的影响
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何进1 , 王明忠1, 陈志鸿1, 李书志1, 许银生2, 陆平2
作者信息
  • 1．咸宁南玻光电玻璃有限公司，湖北 咸宁 437100
  • 2．硅酸盐建筑材料国家重点实验室，武汉理工大学，武汉 430070
通讯作者:
陆平（1977—），男，博士，副研究员。
作者简介:

何进（1972—），男，硕士，高级工程师。

Effect of Zirconia on Mechanical Properties of Chemically Strengthened Lithium Aluminosilicate Glasses
Jin HE1 , Mingzhong WANG1, Zhihong CHEN1, Shuzhi LI1, Yinsheng XU2, Ping LU2
Affiliations
  • 1.Xianning CSG Photovoltaic Glass Co., Ltd., Xianning 437100, Hubei, China
  • 2.State Key Laboratory of Silicate Materials for Architecture, Wuhan University of Technology, Wuhan 430070, China
    • Corresponding Author:
    LU Ping (1977-), male, Ph.D., Associate Professor. E-mail:

    HE Jin (1972-), male, Master, Senior Engineer. E-mail:

出版时间: 2022-02-20 doi: 10.14062/j.issn.0454-5648.20210182
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摘要
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采用熔融淬冷法制备了含不同摩尔分数ZrO2的锂铝硅酸盐玻璃，通过两步化学强化法对玻璃样片进行了化学强化，研究了ZrO2对玻璃的稳定性、硬度和化学强化效果的影响。结果表明：随着ZrO2的摩尔分数从0增加至5%，玻璃化转变温度随之升高，玻璃稳定无析晶现象。引入适量的ZrO2会促进Li+-Na+离子交换，提高应力层深度，表面压应力随着ZrO2浓度的增加而增加，并在摩尔分数为4%时达到最大值，为1 055.6 MPa。中心张应力随着ZrO2浓度的增加先增加后缓慢减小，表明该系列样品具有较好的抗冲击能力。ZrO2的浓度变化对强化后玻璃的硬度影响较小，在引入ZrO2后其抗裂性有所降低，但仍具有较好的抗裂能力。

化学强化  /  盖板玻璃  /  碱铝硅酸盐玻璃  /  氧化锆

Lithium-aluminosilicate glasses with different zirconia (ZrO2) concentrations were prepared by a melting-quenching method. Glass slices were treated using a two-step chemical strengthening method below glass transition temperature (Tg). The effect of ZrO2 addition on the glass stability, hardness and chemical strengthening performance was investigated. The results show that the Tg increases with the increase of ZrO2 concentration in the range of 0-5% (in mole fraction). The absence of crystallization peaks indicates these glasses are rather stable. An appropriate addition of ZrO2 can promote the Li+-Na+ ions exchange and increase the layer depth. The surface compression stress (σc) increases with the increase of the ZrO2 concentration and reaches a maximum value of 1 055.6 MPa at 4% ZrO2 concentration. The center tension firstly increases and then decreases slightly with the increase of the ZrO2 concentration, indicating that these glass samples have a good shock resistance. The addition of ZrO2 has little effect on the hardness of glasses after chemical strengthening. Although the addition of ZrO2 decreases the crack resistance, these glasses still have a good crack resistance performance after chemical strengthening.

chemical strengthening  /  cover glass  /  lithium aluminosilicate glass  /  zirconia
何进, 王明忠, 陈志鸿, 李书志, 许银生, 陆平. 氧化锆对锂铝硅酸盐玻璃化学强化性能的影响. 硅酸盐学报, 2022 , 50 (2) : 372 -377 . DOI: 10.14062/j.issn.0454-5648.20210182
Jin HE, Mingzhong WANG, Zhihong CHEN, Shuzhi LI, Yinsheng XU, Ping LU. Effect of Zirconia on Mechanical Properties of Chemically Strengthened Lithium Aluminosilicate Glasses[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (2) : 372 -377 . DOI: 10.14062/j.issn.0454-5648.20210182
基金
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  • 国家自然科学基金项目(61975156)
  • 咸宁南玻光电玻璃有限公司项目(XNGDJS202007001)
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doi: 10.14062/j.issn.0454-5648.20210182
  • 接收时间：2021-03-15
  • 首发时间：2026-10-22
  • 出版时间：2022-02-20
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  • 收稿日期：2021-03-15
  • 修回日期：2021-06-25
基金
国家自然科学基金项目(61975156)
咸宁南玻光电玻璃有限公司项目(XNGDJS202007001)
作者信息
    1．咸宁南玻光电玻璃有限公司，湖北 咸宁 437100
    2．硅酸盐建筑材料国家重点实验室，武汉理工大学，武汉 430070

通讯作者:

陆平（1977—），男，博士，副研究员。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20210182
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2种不同金属材料的力学参数
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Number of
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Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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