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Article(id=1322942681034403935, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942634976752425, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210128, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1613318400000, receivedDateStr=2021-02-15, revisedDate=1615046400000, revisedDateStr=2021-03-07, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343714245, onlineDateStr=2026-10-30, pubDate=1626710400000, pubDateStr=2021-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343714245, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343714245, creator=13701087609, updateTime=1793343714245, updator=13701087609, issue=Issue{id=1322942634976752425, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='7', pageStart='1249', pageEnd='1518', issueExtLink='null', onlineDate='null', pubDate='1626710400000', pubDateStr='2021-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343703264, creator='13701087609', updateTime=1793345819416, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951510828659213, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942634976752425, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951510828659214, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942634976752425, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1412, endPage=1419, ext={EN=ArticleExt(id=1322942681260896352, articleId=1322942681034403935, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Adsorption Behavior of Mesoporous Silica MCM-41 Derived from Organo-silicone Waste Residue, columnId=1322942641213682516, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Mineral Material, runingTitle=null, highlight=null, articleAbstract=

Organic silicon waste residue was used as silicon source to prepare MCM-41 mesoporous silica by using alkali fusion and hydrothermal reaction method. The effect of alkali fusion time and liquid-solid ratio on extraction rate of the silicon source was evaluated, while the effect of CTAB/SiO2 molar ratio on structure of the mesoporous silica was detailly explored. Besides, adsorption performance of the MCM-41 toward Rhodamine B (RhB) was comprehensively studied. It was found that the MCM-41 possessed highest degree of ordered mesoporous structure, after calcining for 2 h, with the liquid-solid ratio of 50∶1 mL/g, and CTAB/SiO2 molar ratio of 1∶0.3. Accordingly, the specific surface area, pore size and pore volume of the sample were 783.23 m2/g, 2.529 nm and 0.7479 cm3/g, respectively. In addition, the RhB could be effectively removed with MCM-41, with the maximum efficiency to be 295.23 mg/g. Isotherm and kinetic studies revealed that the RhB removal process could be well fitted with Langmuir and pseudo-second-order kinetic models. Meanwhile, owing to its spontaneous and exothermic adsorption, MCM-41 exhibited a high recyclability.

, authors=Yue CAI1, Siyin ZHENG1, Yan HU2, Lingjie ZHANG1, Zhongbang ZHU1, Ping ZHANG1, authorsList=Yue CAI, Siyin ZHENG, Yan HU, Lingjie ZHANG, Zhongbang ZHU, Ping ZHANG, authorCompany=null, correspAuthors=Ping ZHANG, authorNote=

CAI Yue (1998-), female, Master. E-mail:

, correspAuthorsNote=
ZHANG Ping (1981-), female, Ph.D., Associate professor. E-mail:
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942681516748897, articleId=1322942681034403935, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=以有机硅废渣为原料制备介孔二氧化硅MCM-41及其吸附性能, columnId=1322942641389843286, journalTitle=硅酸盐学报, columnName=矿物材料专题, runingTitle=null, highlight=null, articleAbstract=

以有机硅废渣作为硅源，利用碱熔与水热合成相结合的方法制备介孔二氧化硅MCM-41，研究了碱熔时间及液固比对硅源提取率的影响，CTAB/SiO2摩尔比对合成二氧化硅形貌的影响，并考察了MCM-41对水体罗丹明B（RhB）的吸附性能。结果表明：在碱熔时间2 h、液固比50∶1 mL/g、CTAB/SiO2摩尔比1∶0.3条件下合成的介孔二氧化硅MCM-41的介孔结构有序性好，比表面积为783.23 m2/g，孔径和孔容分别为2.529 nm和0.7479 cm3/g。MCM-41对RhB具有较强吸附能力，最大吸附容量为295.23 mL/g，吸附过程符合准二级动力学模型，吸附等温线符合Langmuir单分子层吸附，属自发的放热反应。此外，MCM-41具有良好的吸附再生能力。

, authors=蔡悦1, 郑斯尹1, 胡艳2, 张凌杰1, 朱衷榜1, 章萍1, authorsList=蔡悦, 郑斯尹, 胡艳, 张凌杰, 朱衷榜, 章萍, authorCompany=null, correspAuthors=章萍, authorNote=

蔡悦（1998—），女，硕士研究生。

, correspAuthorsNote=
章萍（1981—），女，博士，副研究员。
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CAI Yue (1998-), female, Master. E-mail:

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蔡悦（1998—），女，硕士研究生。

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蔡悦（1998—），女，硕士研究生。

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以有机硅废渣为原料制备介孔二氧化硅MCM-41及其吸附性能
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蔡悦 1 , 郑斯尹 1 , 胡艳 2 , 张凌杰 1 , 朱衷榜 1 , 章萍 1
硅酸盐学报 | 矿物材料专题 2021,49(7): 1412-1419
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硅酸盐学报 |矿物材料专题 2021 , 49 (7) : 1412 -1419
以有机硅废渣为原料制备介孔二氧化硅MCM-41及其吸附性能
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蔡悦1 , 郑斯尹1, 胡艳2, 张凌杰1, 朱衷榜1, 章萍1
作者信息
  • 1．南昌大学资源环境与化工学院，鄱阳湖环境与资源利用教育部重点实验室，南昌 330047
  • 2．赣州市畜牧研究所，江西 赣州 341401
通讯作者:
章萍（1981—），女，博士，副研究员。
作者简介:

蔡悦（1998—），女，硕士研究生。

Preparation and Adsorption Behavior of Mesoporous Silica MCM-41 Derived from Organo-silicone Waste Residue
Yue CAI1 , Siyin ZHENG1, Yan HU2, Lingjie ZHANG1, Zhongbang ZHU1, Ping ZHANG1
Affiliations
  • 1.Key Laboratory of Environment and Resource Utilization of Poyang Lake and Resource Utilization, Ministry of Education, School of Resource Environment and Chemical Engineering, Nanchang University, Nanchang 330047, China
  • 2.Ganzhou Institute of Animal Science, Ganzhou, 341401, Jiangxi, China
    • Corresponding Author:
    ZHANG Ping (1981-), female, Ph.D., Associate professor. E-mail:

    CAI Yue (1998-), female, Master. E-mail:

出版时间: 2021-07-20 doi: 10.14062/j.issn.0454-5648.20210128
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以有机硅废渣作为硅源，利用碱熔与水热合成相结合的方法制备介孔二氧化硅MCM-41，研究了碱熔时间及液固比对硅源提取率的影响，CTAB/SiO2摩尔比对合成二氧化硅形貌的影响，并考察了MCM-41对水体罗丹明B（RhB）的吸附性能。结果表明：在碱熔时间2 h、液固比50∶1 mL/g、CTAB/SiO2摩尔比1∶0.3条件下合成的介孔二氧化硅MCM-41的介孔结构有序性好，比表面积为783.23 m2/g，孔径和孔容分别为2.529 nm和0.7479 cm3/g。MCM-41对RhB具有较强吸附能力，最大吸附容量为295.23 mL/g，吸附过程符合准二级动力学模型，吸附等温线符合Langmuir单分子层吸附，属自发的放热反应。此外，MCM-41具有良好的吸附再生能力。

有机硅废渣  /  MCM-41  /  水热合成  /  吸附

Organic silicon waste residue was used as silicon source to prepare MCM-41 mesoporous silica by using alkali fusion and hydrothermal reaction method. The effect of alkali fusion time and liquid-solid ratio on extraction rate of the silicon source was evaluated, while the effect of CTAB/SiO2 molar ratio on structure of the mesoporous silica was detailly explored. Besides, adsorption performance of the MCM-41 toward Rhodamine B (RhB) was comprehensively studied. It was found that the MCM-41 possessed highest degree of ordered mesoporous structure, after calcining for 2 h, with the liquid-solid ratio of 50∶1 mL/g, and CTAB/SiO2 molar ratio of 1∶0.3. Accordingly, the specific surface area, pore size and pore volume of the sample were 783.23 m2/g, 2.529 nm and 0.7479 cm3/g, respectively. In addition, the RhB could be effectively removed with MCM-41, with the maximum efficiency to be 295.23 mg/g. Isotherm and kinetic studies revealed that the RhB removal process could be well fitted with Langmuir and pseudo-second-order kinetic models. Meanwhile, owing to its spontaneous and exothermic adsorption, MCM-41 exhibited a high recyclability.

silicone waste residue  /  MCM-41  /  hydrothermal  /  adsorption
蔡悦, 郑斯尹, 胡艳, 张凌杰, 朱衷榜, 章萍. 以有机硅废渣为原料制备介孔二氧化硅MCM-41及其吸附性能. 硅酸盐学报, 2021 , 49 (7) : 1412 -1419 . DOI: 10.14062/j.issn.0454-5648.20210128
Yue CAI, Siyin ZHENG, Yan HU, Lingjie ZHANG, Zhongbang ZHU, Ping ZHANG. Preparation and Adsorption Behavior of Mesoporous Silica MCM-41 Derived from Organo-silicone Waste Residue[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (7) : 1412 -1419 . DOI: 10.14062/j.issn.0454-5648.20210128
基金
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  • 国家自然科学基金(21767018)
  • 江西省主要学科学术带头人培养项目(20194BCJ22002)
  • 江西省重点研发计划项目(20192BBG70054)
  • 江西省自然科学基金面上项目(2020BAB203013)
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doi: 10.14062/j.issn.0454-5648.20210128
  • 接收时间：2021-02-15
  • 首发时间：2026-10-30
  • 出版时间：2021-07-20
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  • 收稿日期：2021-02-15
  • 修回日期：2021-03-07
基金
国家自然科学基金(21767018)
江西省主要学科学术带头人培养项目(20194BCJ22002)
江西省重点研发计划项目(20192BBG70054)
江西省自然科学基金面上项目(2020BAB203013)
作者信息
    1．南昌大学资源环境与化工学院，鄱阳湖环境与资源利用教育部重点实验室，南昌 330047
    2．赣州市畜牧研究所，江西 赣州 341401

通讯作者:

章萍（1981—），女，博士，副研究员。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20210128
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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