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Article(id=1322942879592755928, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210049, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1610726400000, receivedDateStr=2021-01-16, revisedDate=1614528000000, revisedDateStr=2021-03-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343761585, onlineDateStr=2026-10-30, pubDate=1634659200000, pubDateStr=2021-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343761585, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343761585, creator=13701087609, updateTime=1793343761585, updator=13701087609, issue=Issue{id=1322942849381183980, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='10', pageStart='2045', pageEnd='2312', issueExtLink='null', onlineDate='null', pubDate='1634659200000', pubDateStr='2021-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343754382, creator='13701087609', updateTime=1793345931656, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951981580562527, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951981584756832, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2098, endPage=2105, ext={EN=ArticleExt(id=1322942880851047129, articleId=1322942879592755928, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Performance of Mordenite Membranes by SiO2-ZrO2 Sol Modified Seed Method, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The integrity of the seed layer was improved by adding SiO2-ZrO2 nano-sized sol into the seed solution on macroporous α-Al2O3 carrier for the preparation of high-performance mordenite membranes. The effect of SiO2-ZrO2 sol amount added in the seed crystal on the seed layer and zeolite membrane was investigated. The results show that the pervaporation performance of mordenite membranes is improved by the addition of SiO2-ZrO2 sols. The flux and separation factor decreases slightly as the concentration increases. When 0.5% (in mass fraction) SiO2-ZrO2 sol is added into the seed crystal, the permeation flux and separation factor can reach 0.94 kg/(m2·h) and 5 285 by a pervaporation of 90% (in mass fraction) acetic acid/water solution at 75℃. It is indicated that SiO2-ZrO2 sol improves the dispersion of the seed in the solution. The mordenite membrane prepared by this method has good repeatability and acid resistance.

, authors=Ming DING1, Xiuxiu REN1, Nanhua WU1, Lanpeng LI2, Quan ZHANG2, Rong XU1, Jing ZHONG1, authorsList=Ming DING, Xiuxiu REN, Nanhua WU, Lanpeng LI, Quan ZHANG, Rong XU, Jing ZHONG, authorCompany=null, correspAuthors=Xiuxiu REN, Jing ZHONG, authorNote=

DING Ming (1996-), female, Master candidate. E-mail:

, correspAuthorsNote=
ZHONG Jing (1972-), female, Ph.D., Professor; E-mail:
REN Xiuxiu(1987-), female, Ph.D., Lecturer.
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通过在晶种液中引入多羟基的SiO2-ZrO2纳米溶胶，提高在大孔α-Al2O3载体上晶种层的连续性，从而制备出高性能的丝光沸石膜。研究了晶种中SiO2-ZrO2溶胶的添加量对晶种层及沸石膜的影响。结果表明：在晶种中添加SiO2-ZrO2溶胶制备的丝光沸石膜与未添加的相比，均表现了较高分离性能。随着含量的增加，通量和分离因子稍有下降。当晶种中添加0.5%（质量分数）的SiO2-ZrO2溶胶时，75℃渗透汽化分离90%（质量分数）的乙酸/水溶液，渗透通量和分离因子可分别达到0.94 kg/（m2·h）和5 285。通过电势测定发现SiO2-ZrO2溶胶还增加了晶种在溶液中的分散性。利用该方法制备的丝光沸石膜具有较好的重复性，平均通量为0.93 kg/（m2·h），渗透侧水含量均在99.8%（质量分数）以上，且在100 h的渗透汽化测试中性能保持稳定。

, authors=丁明1, 任秀秀1, 吴楠桦1, 李澜鹏2, 张全2, 徐荣1, 钟璟1, authorsList=丁明, 任秀秀, 吴楠桦, 李澜鹏, 张全, 徐荣, 钟璟, authorCompany=null, correspAuthors=任秀秀, 钟璟, authorNote=

丁明（1996—），女，硕士研究生。

, correspAuthorsNote=
钟璟（1972—），女，博士，教授；
任秀秀（1987—），女，博士，讲师。
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DING Ming (1996-), female, Master candidate. E-mail:

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丁明（1996—），女，硕士研究生。

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SiO2-ZrO2溶胶修饰晶种法制备丝光沸石膜及性能
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丁明 1 , 任秀秀 1 , 吴楠桦 1 , 李澜鹏 2 , 张全 2 , 徐荣 1 , 钟璟 1
硅酸盐学报 | 2021,49(10): 2098-2105
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硅酸盐学报 | 2021 , 49 (10) : 2098 -2105
SiO2-ZrO2溶胶修饰晶种法制备丝光沸石膜及性能
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丁明（1996—），女，硕士研究生。

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丁明1 , 任秀秀1 , 吴楠桦1, 李澜鹏2, 张全2, 徐荣1, 钟璟1
作者信息
  • 1．常州大学石油化工学院，江苏省绿色催化材料与技术重点实验室，江苏 常州 213164
  • 2．中国石油化工股份有限公司，大连石油化工研究院，辽宁 大连 116000
通讯作者:
钟璟（1972—），女，博士，教授；
任秀秀（1987—），女，博士，讲师。
作者简介:

丁明（1996—），女，硕士研究生。

Preparation and Performance of Mordenite Membranes by SiO2-ZrO2 Sol Modified Seed Method
Ming DING1 , Xiuxiu REN1 , Nanhua WU1, Lanpeng LI2, Quan ZHANG2, Rong XU1, Jing ZHONG1
Affiliations
  • 1.Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology, School of Petrochemical Engineering, Changzhou University, Changzhou 213164, Jiangsu, China
  • 2.China Petrochemical Corporation, Dalian Petrochemical Research Institute, Dalian 116000, Liaoning, China
    • Corresponding Author:
    ZHONG Jing (1972-), female, Ph.D., Professor; E-mail:
    REN Xiuxiu(1987-), female, Ph.D., Lecturer.

    DING Ming (1996-), female, Master candidate. E-mail:

出版时间: 2021-10-20 doi: 10.14062/j.issn.0454-5648.20210049
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通过在晶种液中引入多羟基的SiO2-ZrO2纳米溶胶，提高在大孔α-Al2O3载体上晶种层的连续性，从而制备出高性能的丝光沸石膜。研究了晶种中SiO2-ZrO2溶胶的添加量对晶种层及沸石膜的影响。结果表明：在晶种中添加SiO2-ZrO2溶胶制备的丝光沸石膜与未添加的相比，均表现了较高分离性能。随着含量的增加，通量和分离因子稍有下降。当晶种中添加0.5%（质量分数）的SiO2-ZrO2溶胶时，75℃渗透汽化分离90%（质量分数）的乙酸/水溶液，渗透通量和分离因子可分别达到0.94 kg/（m2·h）和5 285。通过电势测定发现SiO2-ZrO2溶胶还增加了晶种在溶液中的分散性。利用该方法制备的丝光沸石膜具有较好的重复性，平均通量为0.93 kg/（m2·h），渗透侧水含量均在99.8%（质量分数）以上，且在100 h的渗透汽化测试中性能保持稳定。

丝光沸石膜  /  二氧化硅-氧化锆溶胶  /  晶种层  /  渗透汽化

The integrity of the seed layer was improved by adding SiO2-ZrO2 nano-sized sol into the seed solution on macroporous α-Al2O3 carrier for the preparation of high-performance mordenite membranes. The effect of SiO2-ZrO2 sol amount added in the seed crystal on the seed layer and zeolite membrane was investigated. The results show that the pervaporation performance of mordenite membranes is improved by the addition of SiO2-ZrO2 sols. The flux and separation factor decreases slightly as the concentration increases. When 0.5% (in mass fraction) SiO2-ZrO2 sol is added into the seed crystal, the permeation flux and separation factor can reach 0.94 kg/(m2·h) and 5 285 by a pervaporation of 90% (in mass fraction) acetic acid/water solution at 75℃. It is indicated that SiO2-ZrO2 sol improves the dispersion of the seed in the solution. The mordenite membrane prepared by this method has good repeatability and acid resistance.

mordenite membrane  /  silica-zirconia sol  /  seed layer  /  pervaporation
丁明, 任秀秀, 吴楠桦, 李澜鹏, 张全, 徐荣, 钟璟. SiO2-ZrO2溶胶修饰晶种法制备丝光沸石膜及性能. 硅酸盐学报, 2021 , 49 (10) : 2098 -2105 . DOI: 10.14062/j.issn.0454-5648.20210049
Ming DING, Xiuxiu REN, Nanhua WU, Lanpeng LI, Quan ZHANG, Rong XU, Jing ZHONG. Preparation and Performance of Mordenite Membranes by SiO2-ZrO2 Sol Modified Seed Method[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (10) : 2098 -2105 . DOI: 10.14062/j.issn.0454-5648.20210049
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  • 中国石油化工股份有限公司科技项目(420037)
  • 江苏省自然科学基金(BK20200982)
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2021年第49卷第10期
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doi: 10.14062/j.issn.0454-5648.20210049
  • 接收时间：2021-01-16
  • 首发时间：2026-10-30
  • 出版时间：2021-10-20
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  • 收稿日期：2021-01-16
  • 修回日期：2021-03-01
基金
中国石油化工股份有限公司科技项目(420037)
江苏省自然科学基金(BK20200982)
作者信息
    1．常州大学石油化工学院，江苏省绿色催化材料与技术重点实验室，江苏 常州 213164
    2．中国石油化工股份有限公司，大连石油化工研究院，辽宁 大连 116000

通讯作者:

钟璟（1972—），女，博士，教授；
任秀秀（1987—），女，博士，讲师。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20210049
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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