Article(id=1322943502530781833, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200973, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1609084800000, receivedDateStr=2020-12-28, revisedDate=1613664000000, revisedDateStr=2021-02-19, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343910105, onlineDateStr=2026-10-30, pubDate=1632067200000, pubDateStr=2021-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343910105, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343910105, creator=13701087609, updateTime=1793343910105, updator=13701087609, issue=Issue{id=1322942780003201932, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='9', pageStart='1785', pageEnd='2044', issueExtLink='null', onlineDate='null', pubDate='1632067200000', pubDateStr='2021-09-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343737841, creator='13701087609', updateTime=1793345873558, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951737916665918, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951737916665919, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2017, endPage=2024, ext={EN=ArticleExt(id=1322943502782440074, articleId=1322943502530781833, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Thermal Insulation Property of Yolk-shell Structure Hollow Silica Nanospheres, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

Yolk-shell structure hollow silica nanospheres were prepared with TEOS as a silica precursor and polystyrene sphere as a template by a continuous hard-template wrapping synthesis method and subsequent high temperature calcining. The structure, morphology and properties of the as-synthesized products were characterized by zeta potential analysis, Fourier transform infrared spectroscopy, scanning electron microscopy, transmission electron microscopy, nitrogen adsorption-desorption isotherm and thermal conductivity analysis. The thermal insulation properties of acrylate coating with yolk-shell structure hollow silica nanospheres were investigated. The results show yolk-shell structure hollow silica nanospheres with 20-290 nm layer space have a petal-like morphology. The thermal conductivity is 0.0500-0.0650 W·m^-1·K^-1, which increases with the increase of inner core particle size. The incorporation of yolk-shell structure hollow silica nanospheres into acrylate coating can effectively reduce the thermal conductivity of the coating, which can be reduced by more than 70% at the incorporation content of 8%. Compared to single shell hollow silica nanospheres, yolk-shell structure hollow silica nanospheres have a decreased thermal conductivity of the coating and a better thermal insulation performance.

, authors=Fangxian LI, Yerong YANG, Jiangxiong WEI, Qijun YU, authorsList=Fangxian LI, Yerong YANG, Jiangxiong WEI, Qijun YU, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943503046681227, articleId=1322943502530781833, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=蛋黄-蛋壳型中空纳米SiO₂微球的制备及绝热性能, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

以正硅酸乙酯为硅源和聚苯乙烯球为牺牲模板，采用连续硬模板包裹法结合后续高温煅烧技术制备了蛋黄-蛋壳型中空纳米SiO₂微球。通过表面电位分析、Fourier变换红外光谱、扫描电子显微镜、透射电子显微镜、氮气吸附-脱附、热常数分析等手段对制备得到的中空纳米SiO₂微球进行结构、微观形貌和性能表征，将蛋黄-蛋壳型中空纳米SiO₂微球应用于丙烯酸酯隔热涂层中考察其绝热性能。研究表明：蛋黄-蛋壳型中空纳米SiO₂形貌呈花瓣状，壳层间距在20~290 nm，随着内核尺寸的增大，比表面积逐渐减小；蛋黄-蛋壳型中空纳米SiO₂微球的热导率的范围在0.0500~0.0650 W·m^-1·K^-1之间，随着内核粒径的增加，热导率逐渐增大；中空纳米SiO₂可以有效降低涂层的热导率，当掺量为8%时，热导率降低70%以上；相比单壳层中空纳米SiO₂，蛋黄-蛋壳结构中空纳米SiO₂能更有效降低涂层的热导率，具有更好的绝热性能。

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LI Fangxian (1979-), male, Ph.D., Associate Researcher E-mail: msfxli@scut.edu.cn

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李方贤（1979—），男，博士，副研究员。

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李方贤（1979—），男，博士，副研究员。

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