Article(id=1322943575029326013, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200918, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1607616000000, receivedDateStr=2020-12-11, revisedDate=1609689600000, revisedDateStr=2021-01-04, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343927388, onlineDateStr=2026-10-30, pubDate=1634659200000, pubDateStr=2021-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343927388, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343927388, creator=13701087609, updateTime=1793343927388, updator=13701087609, issue=Issue{id=1322942849381183980, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='10', pageStart='2045', pageEnd='2312', issueExtLink='null', onlineDate='null', pubDate='1634659200000', pubDateStr='2021-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343754382, creator='13701087609', updateTime=1793345931656, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951981580562527, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951981584756832, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2276, endPage=2285, ext={EN=ArticleExt(id=1322943575213875390, articleId=1322943575029326013, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Compositional-structural Gradient Change of C(N)-A-S-H(I) Gel in Alkali-activated Slag after Magnesium Sulphate Attack, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

This paper presented the gradient changes of the characteristics of C(N)-A-S-H (Calcium(Sodium)-Aluminium-Silicate Hydrates) gel in alkali-activated slag (AAS) mortars subjected to sulphate attack in 10% (in mass fraction) MgSO₄ solution by ²⁹Si solid-state magic-angle Spinning nuclear magnetic resonance (SS MAS-NMR), and high-resolution transmission electron microscopy-energy dispersive X-ray spectroscopy (HR TEM-EDX). The results show that the outer layer with the thickness of 0.5-3 mm after attack is mainly composed of Si-Al gel, the middle-level layer with the thickness of 3-6 mm is M/C(N)-A-S-H gel, and the internal layer with the thickness of 6-9 mm is mainly composed of C(N)-A-S-H gel (which was almost not attacked. The stable crystal tobermorite (Ca/Si ratio=0.98) and hydrotalcite-like phase (Mg/Al ratio=2.39) could not be destroyed by sulphate attack. However, the main chain of C(N)-A-S-H gel is readily attacked by sulphate at [AlO₄] bridging tetrahedra (BT). Meanwhile, the magnesium sulphate initially results in de-calcium phenomenon (Mg will replace Ca), and then generates the de-aluminium phenomenon, finally forming the Si-Al gel (main product in the out layer) when removing Ca and partial Al from the gel and charge-balancing the gel by abundant Mg ions.

, authors=Xiaohong ZHU^{1, 2}, Qing LI^{1, 3}, Deyi XIONG³, Kai YANG³, Changhui YANG³, Rongjin LIU¹, authorsList=Xiaohong ZHU, Qing LI, Deyi XIONG, Kai YANG, Changhui YANG, Rongjin LIU, authorCompany=null, correspAuthors=Qing LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943575629111487, articleId=1322943575029326013, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=硫酸镁侵蚀后碱矿渣水泥中C(N)-A-S-H(I)组成-结构梯度变化, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

通过²⁹Si魔角自旋核磁共振及高分辨透射电镜-能谱方法，研究了10%（质量分数）硫酸镁溶液侵蚀后碱矿渣水泥（AAS）砂浆中C（N）-A-S-H凝胶结构梯度变化。结果表明：侵蚀表层（0.5~3.0 mm）主要为硅铝凝胶；侵蚀中层（3~6 mm）主要为M/C（N）-A-S-H凝胶；内部（6~9 mm）主要为C（N）-A-S-H凝胶（几乎未受到侵蚀）；在硫酸盐侵蚀后仍会有稳定的类托贝莫来石（Ca/Si摩尔比为0.98）/类水滑石（Mg/Al摩尔比为2.39）晶体存在，但C（N）-A-S-H凝胶主链中，位于桥氧四面体（BT）位置的铝氧四面体受硫酸盐侵蚀影响更大。同时，硫酸镁侵蚀首先造成脱钙现象发生（其位置将会由Mg补充），而后产生脱铝现象，当C-A-S-H完成脱Ca及部分脱Al后，形成Al-Si凝胶且凝胶中存在大量Mg平衡离子（即最外层产物）。

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