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Article(id=1322942771446821694, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942707957641522, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200893, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1606665600000, receivedDateStr=2020-11-30, revisedDate=1608134400000, revisedDateStr=2020-12-17, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343735800, onlineDateStr=2026-10-30, pubDate=1629388800000, pubDateStr=2021-08-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343735800, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343735800, creator=13701087609, updateTime=1793343735800, updator=13701087609, issue=Issue{id=1322942707957641522, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='8', pageStart='1519', pageEnd='1784', issueExtLink='null', onlineDate='null', pubDate='1629388800000', pubDateStr='2021-08-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343720664, creator='13701087609', updateTime=1793345848275, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951631859494962, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942707957641522, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951631859494963, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942707957641522, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1543, endPage=1549, ext={EN=ArticleExt(id=1322942771669119808, articleId=1322942771446821694, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Acid Leaching on Structure and Properties of High Silica Glass Fibers, columnId=1322942708590981427, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Functional Glass, runingTitle=null, highlight=null, articleAbstract=

The morphology and structure of fiber precursors before and after acid leaching were characterized by scanning electron microscopy (SEM) and infrared spectroscopy (IR), and the Na+ leaching process was characterized by inductively coupled plasma spectrometry (ICP). The effects of hydrochloric acid concentration, leaching temperature and time on the leaching rate of Na+ and mechanical properties of the fiber precursor were investigated. The Na+ leaching rate reaches 85% after leaching in 3 mol/L hydrochloric acid solution for 12 h at 90℃. The maximum strength retention rate of the fiber after leaching can be obtained when the concentration of hydrochloric acid is 5 mol/L. In this case, Na+ ions in the fiber are replaced with H+ ions in hydrochloric acid during the acid leaching process, whereas hydroxyl group is further polymerized and dehydrated, thus strengthening the glass network during the heat treatment process and improving the fiber strength.

, authors=Shuaiming ZHANG1, 2, 3, Lida LUO1, 2, 3, Linfeng DING1, 2, 3, Zhengwei LIU1, 2, 3, Weizhong JIANG1, 2, 3, Qingwei WANG1, 2, 3, 4, authorsList=Shuaiming ZHANG, Lida LUO, Linfeng DING, Zhengwei LIU, Weizhong JIANG, Qingwei WANG, authorCompany=null, correspAuthors=Qingwei WANG, authorNote=

ZHANG Shuaiming (1996-), male, Master candidate. E-mail:

, correspAuthorsNote=
WANG Qingwei (1978-), male, Associate Professor. E-mail:
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942771937555265, articleId=1322942771446821694, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=酸沥滤对高硅氧玻璃纤维结构及性能的影响, columnId=1322942708762947893, journalTitle=硅酸盐学报, columnName=功能玻璃专题, runingTitle=null, highlight=null, articleAbstract=

通过扫描电子显微镜和红外光谱仪观察纤维前驱体酸沥滤前后的形貌和结构变化，通过ICP分析Na+的沥出过程，研究了盐酸浓度、温度以及沥滤时间对纤维前驱体Na+沥出率及力学性能的影响。结果表明：高硅氧纤维前驱体在90℃的3 mol/L盐酸溶液中沥滤12 h后，纤维中的Na+沥出率达到85%以上；当盐酸浓度为5 mol/L时，沥滤后纤维的强度保留率最高。在酸沥滤过程中纤维中的Na+与盐酸中的H+置换，在热处理过程中羟基进一步聚合脱水补强玻璃网络体，实现纤维强度的提升。

, authors=张帅明1, 2, 3, 罗理达1, 2, 3, 丁林锋1, 2, 3, 刘郑威1, 2, 3, 蒋伟忠1, 2, 3, 汪庆卫1, 2, 3, 4, authorsList=张帅明, 罗理达, 丁林锋, 刘郑威, 蒋伟忠, 汪庆卫, authorCompany=null, correspAuthors=汪庆卫, authorNote=

张帅明（1996—），男，硕士研究生。

, correspAuthorsNote=
汪庆卫（1978—），男，博士，副研究员。
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ZHANG Shuaiming (1996-), male, Master candidate. E-mail:

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ZHANG Shuaiming (1996-), male, Master candidate. E-mail:

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2．先进玻璃制造技术教育部工程研究中心，上海 201620
3．中国轻工业特种玻璃及搪瓷重点实验室，上海 201620, bio={"content":"

张帅明（1996—），男，硕士研究生。

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张帅明（1996—），男，硕士研究生。

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2.Engineering Center of Advanced Glass Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China
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2．先进玻璃制造技术教育部工程研究中心，上海 201620
3．中国轻工业特种玻璃及搪瓷重点实验室，上海 201620, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1322942773543973699, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, xref=1., ext=[AuthorCompanyExt(id=1322942773552362308, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, companyId=1322942773543973699, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1.State Key Laboratory for Modification of chemical Fibers and Polymer Materials, Donghua University, Shanghai 201620, China), AuthorCompanyExt(id=1322942773560750917, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, companyId=1322942773543973699, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1．东华大学纤维材料改性国家重点实验室，上海 201620)]), AuthorCompany(id=1322942773623665478, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, xref=2., ext=[AuthorCompanyExt(id=1322942773632054087, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, companyId=1322942773623665478, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.Engineering Center of Advanced Glass Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China), AuthorCompanyExt(id=1322942773636248392, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, companyId=1322942773623665478, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2．先进玻璃制造技术教育部工程研究中心，上海 201620)]), AuthorCompany(id=1322942773749494601, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, xref=3., ext=[AuthorCompanyExt(id=1322942773757883210, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, companyId=1322942773749494601, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3.Key Laboratory of Special Glass and Enamel for China Light Industry, Donghua University, Shanghai 201620, China), AuthorCompanyExt(id=1322942773766271819, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, companyId=1322942773749494601, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3．中国轻工业特种玻璃及搪瓷重点实验室，上海 201620)])]), Author(id=1322942774374445919, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, orderNo=2, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1322942774454137699, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942771446821694, authorId=1322942774374445919, language=EN, stringName=Linfeng DING, firstName=Linfeng, middleName=null, lastName=DING, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, 2, 3, address=1.State Key Laboratory for Modification of chemical Fibers and Polymer Materials, Donghua University, Shanghai 201620, China
2.Engineering Center of Advanced Glass Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China
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2．先进玻璃制造技术教育部工程研究中心，上海 201620
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2.Engineering Center of Advanced Glass Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China
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酸沥滤对高硅氧玻璃纤维结构及性能的影响
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张帅明 1, 2, 3 , 罗理达 1, 2, 3 , 丁林锋 1, 2, 3 , 刘郑威 1, 2, 3 , 蒋伟忠 1, 2, 3 , 汪庆卫 1, 2, 3, 4
硅酸盐学报 | 功能玻璃专题 2021,49(8): 1543-1549
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硅酸盐学报 |功能玻璃专题 2021 , 49 (8) : 1543 -1549
酸沥滤对高硅氧玻璃纤维结构及性能的影响
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张帅明1, 2, 3 , 罗理达1, 2, 3, 丁林锋1, 2, 3, 刘郑威1, 2, 3, 蒋伟忠1, 2, 3, 汪庆卫1, 2, 3, 4
作者信息
  • 1．东华大学纤维材料改性国家重点实验室，上海 201620
  • 2．先进玻璃制造技术教育部工程研究中心，上海 201620
  • 3．中国轻工业特种玻璃及搪瓷重点实验室，上海 201620
  • 4．临沂昊泉硅业科技有限公司，山东 临沂 276003
通讯作者:
汪庆卫（1978—），男，博士，副研究员。
作者简介:

张帅明（1996—），男，硕士研究生。

Effect of Acid Leaching on Structure and Properties of High Silica Glass Fibers
Shuaiming ZHANG1, 2, 3 , Lida LUO1, 2, 3, Linfeng DING1, 2, 3, Zhengwei LIU1, 2, 3, Weizhong JIANG1, 2, 3, Qingwei WANG1, 2, 3, 4
Affiliations
  • 1.State Key Laboratory for Modification of chemical Fibers and Polymer Materials, Donghua University, Shanghai 201620, China
  • 2.Engineering Center of Advanced Glass Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China
  • 3.Key Laboratory of Special Glass and Enamel for China Light Industry, Donghua University, Shanghai 201620, China
  • 4.Linyi Haoquan Silicon Industry Technology Co.Ltd, Linyi 276003, Shandong, China
    • Corresponding Author:
    WANG Qingwei (1978-), male, Associate Professor. E-mail:

    ZHANG Shuaiming (1996-), male, Master candidate. E-mail:

出版时间: 2021-08-20 doi: 10.14062/j.issn.0454-5648.20200893
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通过扫描电子显微镜和红外光谱仪观察纤维前驱体酸沥滤前后的形貌和结构变化，通过ICP分析Na+的沥出过程，研究了盐酸浓度、温度以及沥滤时间对纤维前驱体Na+沥出率及力学性能的影响。结果表明：高硅氧纤维前驱体在90℃的3 mol/L盐酸溶液中沥滤12 h后，纤维中的Na+沥出率达到85%以上；当盐酸浓度为5 mol/L时，沥滤后纤维的强度保留率最高。在酸沥滤过程中纤维中的Na+与盐酸中的H+置换，在热处理过程中羟基进一步聚合脱水补强玻璃网络体，实现纤维强度的提升。

酸沥滤  /  高硅氧  /  玻璃纤维  /  结构  /  强度

The morphology and structure of fiber precursors before and after acid leaching were characterized by scanning electron microscopy (SEM) and infrared spectroscopy (IR), and the Na+ leaching process was characterized by inductively coupled plasma spectrometry (ICP). The effects of hydrochloric acid concentration, leaching temperature and time on the leaching rate of Na+ and mechanical properties of the fiber precursor were investigated. The Na+ leaching rate reaches 85% after leaching in 3 mol/L hydrochloric acid solution for 12 h at 90℃. The maximum strength retention rate of the fiber after leaching can be obtained when the concentration of hydrochloric acid is 5 mol/L. In this case, Na+ ions in the fiber are replaced with H+ ions in hydrochloric acid during the acid leaching process, whereas hydroxyl group is further polymerized and dehydrated, thus strengthening the glass network during the heat treatment process and improving the fiber strength.

acid leaching  /  high silica  /  glass fiber  /  structure  /  strength
张帅明, 罗理达, 丁林锋, 刘郑威, 蒋伟忠, 汪庆卫. 酸沥滤对高硅氧玻璃纤维结构及性能的影响. 硅酸盐学报, 2021 , 49 (8) : 1543 -1549 . DOI: 10.14062/j.issn.0454-5648.20200893
Shuaiming ZHANG, Lida LUO, Linfeng DING, Zhengwei LIU, Weizhong JIANG, Qingwei WANG. Effect of Acid Leaching on Structure and Properties of High Silica Glass Fibers[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (8) : 1543 -1549 . DOI: 10.14062/j.issn.0454-5648.20200893
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  • 国家自然科学基金面上项目(51873032)
  • 中央高校基础研究项目(223201900003)
  • 山东省重点研发计划(2019JZZY010308)
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2021年第49卷第8期
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doi: 10.14062/j.issn.0454-5648.20200893
  • 接收时间：2020-11-30
  • 首发时间：2026-10-30
  • 出版时间：2021-08-20
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  • 收稿日期：2020-11-30
  • 修回日期：2020-12-17
基金
国家自然科学基金面上项目(51873032)
中央高校基础研究项目(223201900003)
山东省重点研发计划(2019JZZY010308)
作者信息
    1．东华大学纤维材料改性国家重点实验室，上海 201620
    2．先进玻璃制造技术教育部工程研究中心，上海 201620
    3．中国轻工业特种玻璃及搪瓷重点实验室，上海 201620
    4．临沂昊泉硅业科技有限公司，山东 临沂 276003

通讯作者:

汪庆卫（1978—），男，博士，副研究员。
参考文献
分享链接
https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200893
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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