Article(id=1322943198624088181, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200458, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1593014400000, receivedDateStr=2020-06-25, revisedDate=1593878400000, revisedDateStr=2020-07-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343837647, onlineDateStr=2026-10-30, pubDate=1616169600000, pubDateStr=2021-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343837647, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343837647, creator=13701087609, updateTime=1793343837647, updator=13701087609, issue=Issue{id=1322942495801356913, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='3', pageStart='441', pageEnd='604', issueExtLink='null', onlineDate='null', pubDate='1616169600000', pubDateStr='2021-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343670081, creator='13701087609', updateTime=1793345495044, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950150322258738, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950150322258739, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=469, endPage=475, ext={EN=ArticleExt(id=1322943201186807926, articleId=1322943198624088181, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Influence of La-Ho Doping on Microstructure Formation of BiFeO₃, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

BiFeO₃ (BFO) and Bi_0.8La_0.1Ho_0.1FeO₃ (BLHFO) materials were prepared by a solid-state reaction method. The dynamic process of melting and solidification of the samples was observed in real time by high temperature polarizing microscopy. The phase composition, microstructure and element distribution of the solidified samples were analyzed by X-ray diffraction, scanning electron microscopy and energy dispersive spectrometry. It is indicated that BFO and BLHFO samples both have polyhedral Fe₂O₃ grains precipitated along with the melting and further grow in the cooling process. Based on the results by SEM, a continuous Bi₂O₃ phase is mixed with a small amount of micron-sized Fe₂O₃ grains and a large amount of micron-sized BiFeO₃ grains. BiFeO₃ grains in the undoped samples are irregular, while La-Ho doped samples form regular cubic BiFeO₃ crystals. In addition, Fe₂O₃ grains in the co-doped sample only contain La element. La and Ho can be co-doped into BiFeO₃ polyhedral grains.

, authors=Junhuai XIANG¹, Mingfeng LIU¹, Xiuhong PAN², Minghui ZHANG², Xuechao LIU², authorsList=Junhuai XIANG, Mingfeng LIU, Xiuhong PAN, Minghui ZHANG, Xuechao LIU, authorCompany=null, correspAuthors=Xiuhong PAN, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943205762793592, articleId=1322943198624088181, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=La-Ho掺杂对BiFeO₃组织结构形成的影响, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用固相合成方法制备了BiFeO₃（BFO）、Bi_0.8La_0.1Ho_0.1FeO₃（BLHFO）样品，并利用高温偏光显微镜实时观察了样品升温熔化-凝固的动态过程，凝固后的样品通过微焦斑二维衍射仪、扫描电子显微镜及能谱仪分析其物相组成、微观形貌及元素分布。实时观察发现BFO和BLHFO样品升温过程中均呈现边熔化边析出多面体Fe₂O₃晶粒，并在降温过程中进一步长大的现象。凝固后的SEM扫描显示，在连续的Bi₂O₃相中夹杂少量几十微米的Fe₂O₃晶粒，以及大量几微米的BiFeO₃晶粒，未掺杂的样品中BiFeO₃是无规则的，而La-Ho掺杂的样品中形成了规则立方体形状的BiFeO₃晶体。此外，能谱分析还显示，共掺样品中Fe₂O₃晶粒内只含有La元素，而La和Ho元素可以共掺进入BiFeO₃多面体晶粒中。

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XIANG Junhuai (1971-), male, Ph.D., Professor. E-mail: xiangjunhuai@163.com

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XIANG Junhuai (1971-), male, Ph.D., Professor. E-mail: xiangjunhuai@163.com

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向军淮（1971—），男，博士，教授。

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向军淮（1971—），男，博士，教授。

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