Article(id=1322942537580819333, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200450, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1592755200000, receivedDateStr=2020-06-22, revisedDate=1594396800000, revisedDateStr=2020-07-11, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343680043, onlineDateStr=2026-10-30, pubDate=1616169600000, pubDateStr=2021-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343680043, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343680043, creator=13701087609, updateTime=1793343680043, updator=13701087609, issue=Issue{id=1322942495801356913, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='3', pageStart='441', pageEnd='604', issueExtLink='null', onlineDate='null', pubDate='1616169600000', pubDateStr='2021-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343670081, creator='13701087609', updateTime=1793345495044, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950150322258738, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950150322258739, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=590, endPage=596, ext={EN=ArticleExt(id=1322942537777951622, articleId=1322942537580819333, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Phase Composition and Reaction Mechanism of Aluminum-Spinel Composite at 1 700℃ in Flowing Nitrogen, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The phase composition and reaction mechanism of aluminum-spinel (Al-MgAl₂O₄) composite were investigated after being treated at 580℃ for 8 h and 1 700℃ for 3 h in flowing high purity nitrogen. The results show that after being treated at 580℃ for 8 h, the Al-MgAl₂O₄ composite forms an area phenomenon with the aluminum-aluminum nitride (Al-AlN) core-shell structure in the outside area. When the temperature increases up to a critical value, the Al-AlN core-shell structure in the outside area breaks, Al(l/g) reacts with N₂ to form AlN and with O₂ to form Al₂O(g). This process prompts formation of an MgAl₂O₄ spinel with stoichiometric ratio that allows decomposition into Al₂O₃-rich spinel and Mg(g). On the one hand, AlN reacts with Al₂O₃-rich spinel to form MgAlON spinel, and on the other hand, AlN is transformed into (Mg,Al)(N,O) through the solid solution reaction of Mg(g) and O₂(g) into AlN. Phase composition of the inside area is different from the outside area in which MgAlON with flake crystal morphology forms via a gas-gas phase reaction: Al₂O(g)+O₂(g)+N₂(g)+Mg(g)→MgAlON(s) or Al(g)+O₂(g)+N₂(g)+Mg(g)→MgAlON(s) in which Al₂O₃-rich spinel doesn't further form MgAlON spinel.

, authors=Mingwei YAN^{1, 2}, Yumin YANG³, Yong LI⁴, Kaiqi LIU^{1, 2}, Guangchao SUN^{1, 2}, Jiayu ZHANG¹, Chaoquan HU², authorsList=Mingwei YAN, Yumin YANG, Yong LI, Kaiqi LIU, Guangchao SUN, Jiayu ZHANG, Chaoquan HU, authorCompany=null, correspAuthors=Kaiqi LIU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942538004444039, articleId=1322942537580819333, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=1 700℃流动氮气下金属铝-镁铝尖晶石复合材料的物相组成与反应机理, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

研究了高纯氮气下先后进行580℃保温8 h、1 700℃保温3 h热处理后Al-MgAl₂O₄复合材料的物相组成和反应机理。结果表明：经580℃保温8 h后，Al-MgAl₂O₄复合材料形成分层现象，即外层区含金属铝-氮化铝壳核结构。当温度升至某一特定值时，金属铝-氮化铝壳核结构破裂，金属铝Al（l/g）溢出/逸出，与N₂和O₂分别反应生成AlN和Al₂O（g），促进化学计量比的镁铝尖晶石（MgAl₂O₄）分解形成富氧化铝的镁铝尖晶石（Al₂O₃-rich spinel）和镁蒸气（Mg（g））。一方面，AlN与富氧化铝的镁铝尖晶石形成MgAlON尖晶石；另一方面，AlN与Mg（g）和O₂发生固溶体反应生成氮化铝固溶体，（Mg，Al）（N，O）。内层区的材料物相组成不同于外层区，含有许多由气-气反应Al₂O（g）+O₂（g）+N₂（g）+Mg（g）→MgAlON（s）或Al（g）+O₂（g）+N₂（g）+Mg（g）→MgAlON（s）生成的片状MgAlON；此外，内层区富氧化铝的镁铝尖晶石没有进一步转变为MgAlON尖晶石。

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