Article(id=1322943329876443578, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200430, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1592323200000, receivedDateStr=2020-06-17, revisedDate=1596038400000, revisedDateStr=2020-07-30, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343868940, onlineDateStr=2026-10-30, pubDate=1616169600000, pubDateStr=2021-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343868940, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343868940, creator=13701087609, updateTime=1793343868940, updator=13701087609, issue=Issue{id=1322942495801356913, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='3', pageStart='441', pageEnd='604', issueExtLink='null', onlineDate='null', pubDate='1616169600000', pubDateStr='2021-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343670081, creator='13701087609', updateTime=1793345495044, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950150322258738, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950150322258739, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942495801356913, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=441, endPage=447, ext={EN=ArticleExt(id=1322943331231203772, articleId=1322943329876443578, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Co²⁺ Substitution on Microwave Dielectric Properties of Ca₅Mg_4-xCo_x(VO₄)₆ Ceramics, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Ca₅Mg₄(VO₄)₆ microwave dielectric ceramic was prepared by a solid-phase reaction method. Mg element in Ca₅Mg₄(VO₄)₆ ceramic was substituted by Co element in order to improve the microwave dielectric properties. The phase composition and microscopic morphology of the ceramics were determined by X-ray diffraction and scanning electron microscopy. Also, the internal laws of the microwave dielectric properties were analyzed via theoretical calculations, such as bond energy. The formation of solid solution after Co substitutioncan decrease the sintering temperature. The density dominates the change of ε_r at a higher relative density. However, ε_r is mainly affected by the ion polarizability per unit volume at a lower relative density. The grain size reduction caused by the substitution is beneficial to the promotion of the Q×f value. τ_f is closely related to the bond energy and changes with the bond energy of the V—O, which is the maximum bond energy in ceramics. Ca₅Mg₃Co(VO₄)₆ ceramic has the optimum microwave dielectric properties (i.e., ε_r=9.65, Q×f=54 685 GHz, and τ_f = -55.3×10^-6℃^-1).

, authors=Wei LIU¹, Hansheng LENG¹, Bo LI^{1, 2, 3}, authorsList=Wei LIU, Hansheng LENG, Bo LI, authorCompany=null, correspAuthors=Bo LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943333663900101, articleId=1322943329876443578, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=钴离子取代对Ca₅Mg_4-xCo_x(VO₄)₆陶瓷微波介电性能的影响, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用固相反应法制备低温烧结Ca₅Mg₄（VO₄）₆微波介质陶瓷，研究了Co掺杂取代Mg对微波介电性能的影响。结果表明：Co取代后样品形成了固溶体，导致烧结温度降低。当相对密度较低时，致密度主导着ε_r的变化；当相对密度较高时，ε_r主要受单位体积离子极化率的影响。此外，Co取代使得晶粒尺寸减小，进而促进了Q×f值的提升。由于τ_f与键能有着密切的联系，而V—O键的键能最大，τ_f随着V—O键键能的变化而改变。Ca₅Mg₃Co（VO₄）₆具有最佳的微波介电性能：ε_r=9.65，Q×f=54 685 GHz，τ_f=-55.3×10^-6℃^-1。

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LIU Wei (1994-), male, Master candidate. E-mail: gossiple@outlook.com

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LIU Wei (1994-), male, Master candidate. E-mail: gossiple@outlook.com

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刘伟，电子科技大学材料科学与工程硕士研究生，研究方向为低温烧结微波介质陶瓷，研究内容包括微波介质陶瓷的材料设计、制备工艺以及掺杂改性，主要从微波介质陶瓷的微观结构变化入手，同时辅以化学键理论等微观机理，分析陶瓷微观结构的变化对微波介电性能的影响。

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刘伟，电子科技大学材料科学与工程硕士研究生，研究方向为低温烧结微波介质陶瓷，研究内容包括微波介质陶瓷的材料设计、制备工艺以及掺杂改性，主要从微波介质陶瓷的微观结构变化入手，同时辅以化学键理论等微观机理，分析陶瓷微观结构的变化对微波介电性能的影响。

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^2．电子薄膜与集成器件国家重点实验室，成都 610054
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李波，电子科技大学电子科技与工程学院，教授，博士生导师。哈佛大学访问学者，中国电子学会高级会员。主要研究方向为微波陶瓷、微晶玻璃、纳米材料。先后主持国防基础科研重点项目、国防科工局重大项目、装发部预研项目，参与装发部应用开发、装发部重点基金和国家自然科学基金等多个应用基础研究项目。在国内外学术刊物上发表研究论文70余篇，申请国家发明专利20多项。

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李波，电子科技大学电子科技与工程学院，教授，博士生导师。哈佛大学访问学者，中国电子学会高级会员。主要研究方向为微波陶瓷、微晶玻璃、纳米材料。先后主持国防基础科研重点项目、国防科工局重大项目、装发部预研项目，参与装发部应用开发、装发部重点基金和国家自然科学基金等多个应用基础研究项目。在国内外学术刊物上发表研究论文70余篇，申请国家发明专利20多项。

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