Article(id=1322636218450424148, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636193100050547, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200045, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1579622400000, receivedDateStr=2020-01-22, revisedDate=1583337600000, revisedDateStr=2020-03-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270647870, onlineDateStr=2026-10-29, pubDate=1600531200000, pubDateStr=2020-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270647870, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270647870, creator=13701087609, updateTime=1793270647870, updator=13701087609, issue=Issue{id=1322636193100050547, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='9', pageStart='1353', pageEnd='1510', issueExtLink='null', onlineDate='null', pubDate='1594569600000', pubDateStr='2020-07-13', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270641826, creator='13701087609', updateTime=1793270641826, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=1488, endPage=1493, ext={EN=ArticleExt(id=1322636218601419093, articleId=1322636218450424148, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Phase Evolution of Ti-Al₂O₃ Composite Refractory at 1600 ℃ Nitrogen Atmosphere, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Ti-Al₂O₃ composite samples were prepared using sintered alumina and metallic titanium as the raw materials and phenolic resin as the binder. The samples were placed in a graphite crucible and sintered in a carbon tube furnace at 1 600 ℃ in flowing nitrogen. The phase evolution of the sintered samples was analyzed. The results showed that titanium firstly reacted with nitrogen to form titanium nitride. When the content of titanium reached 12%, it can also be fully nitrided. The titanium nitride formed was mostly a flaky structure, and the rest was whisker-like. A small amount of carbon monoxide in nitrogen atmosphere can diffuse into the sample, and form a stable titanium carbonitride solid solution. For samples with 3% titanium, the strength of the sample with 3% graphite decreased by 50%. Similar titanium carbonitride solid solution was formed in Ti-Al₂O₃ samples with and without graphite. Al₅O₆N was found in the corundum sample, but not in Samples with titanium. Alumina can exist stably in the Ti-Al₂O₃ samples with metal titanium added. The phase evolution mechanism model of Ti-Al₂O₃ samples was established.

, authors=Yiming GUO, Yong LI, Yang SUN, Xiaofang WU, Deting XU, Chenhong MA, Xian HE, authorsList=Yiming GUO, Yong LI, Yang SUN, Xiaofang WU, Deting XU, Chenhong MA, Xian HE, authorCompany=null, correspAuthors=Yong LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322636220350443863, articleId=1322636218450424148, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=1600 ℃氮气气氛Ti-Al₂O₃复合耐火材料的相演变行为, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以烧结刚玉和金属钛粉为主要原料、酚醛树脂为结合剂制备Ti-Al₂O₃复合耐火材料样品。将样品置于石墨坩埚中，在碳管炉氮气气氛下1600 ℃烧成。对烧后样品的物相演变进行分析，结果表明：钛与氮气反应形成氮化钛，即使金属钛含量达到12%，也能完全氮化；形成的氮化钛多呈片状，也有一定量的晶须状碳氮化钛固溶体存在。氮气气氛中存在的微量一氧化碳气体扩散到样品内部，最终形成稳定的碳氮化钛固溶体。添加3%金属钛的样品中，添加3%石墨粉后样品强度降低约50%。添加或不添加石墨的Ti-Al₂O₃样品中均形成碳氮化钛固溶体，且碳氮化钛固溶体生成量相近。刚玉样品中出现了Al₅O₆N，在添加钛的样品中未检测到Al₅O₆N。添加金属钛的Ti-Al₂O₃样品中刚玉能稳定存在。建立了Ti-Al₂O₃样品中相演变的演变机理模型。

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GUO Yiming (1995-), female, Master candidate. E-mail: gui987910681@163.com

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GUO Yiming (1995-), female, Master candidate. E-mail: gui987910681@163.com

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郭艺鸣（1995—），女，硕士研究生。

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郭艺鸣（1995—），女，硕士研究生。

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