Article(id=1322612379670655402, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.2020.05.20190429, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1561305600000, receivedDateStr=2019-06-24, revisedDate=1563552000000, revisedDateStr=2019-07-20, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264964262, onlineDateStr=2026-10-29, pubDate=1589904000000, pubDateStr=2020-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264964262, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264964262, creator=13701087609, updateTime=1793264964262, updator=13701087609, issue=Issue{id=1322612265061306700, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='5', pageStart='615', pageEnd='786', issueExtLink='null', onlineDate='null', pubDate='1589904000000', pubDateStr='2020-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264936938, creator='13701087609', updateTime=1793276961694, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662700602208333, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662700602208334, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=723, endPage=729, ext={EN=ArticleExt(id=1322612379830038955, articleId=1322612379670655402, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=In-situ Solvothermal Synthesis and Photocatalytic Performance of TiO2/Ti3C2Tx Composites, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

TiO2/Ti3C2Tx composites were synthesized by a solvothermal method with Ti3C2Tx as substrate and isopropanol (C3H8O) as an inducer. The phase composition and microstructure of TiO2/Ti3C2Tx were characterized by X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy and ultraviolet-visible diffuse reflectance spectroscopy. The results show that anatase type TiO2 is uniformly grown on the layered surface of Ti3C2Tx, thus improving the electron transport performance of TiO2/Ti3C2Tx composites. The optimum photocatalytic performance of TiO2/Ti3C2Tx-24 h can be obtained under the irradiation of 500 W mercury lamp (365 nm UV light), and the degradation efficiency of methyl orange (MO) is 95% for 75 min, which is 67.7% greater than that of pure TiO2 photocatalyst.

, authors=Huiqi ZHENG1, Jin CHEN1, Yang ZHAO1, Wendong WANG2, Xiping LEI1, authorsList=Huiqi ZHENG, Jin CHEN, Yang ZHAO, Wendong WANG, Xiping LEI, authorCompany=null, correspAuthors=Jin CHEN, authorNote=

ZHENG Huiqi (1993-), male, Master candidate. E-mail:

, correspAuthorsNote=
CHEN Jin (1978-), male, Ph.D., Associate Professor. E-mail:
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322612380035559852, articleId=1322612379670655402, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=溶剂热法原位制备TiO2/Ti3C2Tx复合材料及其光催化性能, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以Ti3C2Tx为基底材料,异丙醇(C3H8O)为诱导剂,通过溶剂热法制备TiO2/Ti3C2Tx复合材料。采用X射线衍射、扫描电子显微镜、X射线光电子能谱和紫外可见漫反射光谱对样品物相组成及微观结构进行表征。结果表明:在Ti3C2Tx层状表面均匀生长出锐钛矿晶型的TiO2,所得TiO2/Ti3C2Tx复合材料光生电子传输性能提高。TiO2/Ti3C2Tx-24 h在500 W汞灯(波长为365 nm)照射下其光催化性能最佳,75 min可降解甲基橙(MO)95%,比纯TiO2光催化剂降解效率提高了67.7%。

, authors=郑会奇1, 陈晋1, 赵杨1, 王文东2, 雷西萍1, authorsList=郑会奇, 陈晋, 赵杨, 王文东, 雷西萍, authorCompany=null, correspAuthors=陈晋, authorNote=

郑会奇(1993—),男,硕士研究生。

, correspAuthorsNote=
陈晋(1978—),男,博士,副教授。
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ZHENG Huiqi (1993-), male, Master candidate. E-mail:

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郑会奇(1993—),男,硕士研究生。

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郑会奇(1993—),男,硕士研究生。

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溶剂热法原位制备TiO2/Ti3C2Tx复合材料及其光催化性能
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郑会奇 1 , 陈晋 1 , 赵杨 1 , 王文东 2 , 雷西萍 1
硅酸盐学报 | 2020,48(5): 723-729
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硅酸盐学报 | 2020 , 48 (5) : 723 -729
溶剂热法原位制备TiO2/Ti3C2Tx复合材料及其光催化性能
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郑会奇1 , 陈晋1 , 赵杨1, 王文东2, 雷西萍1
作者信息
  • 1.西安建筑科技大学材料科学与工程学院,西安 710055
  • 2.西安交通大学人居环境与建筑工程学院,西安 710049
通讯作者:
陈晋(1978—),男,博士,副教授。
作者简介:

郑会奇(1993—),男,硕士研究生。

In-situ Solvothermal Synthesis and Photocatalytic Performance of TiO2/Ti3C2Tx Composites
Huiqi ZHENG1 , Jin CHEN1 , Yang ZHAO1, Wendong WANG2, Xiping LEI1
Affiliations
  • 1.College of Materials Science and Engineering, Xi'an University of Architecture and Technology, Xi'an 710055, China
  • 2.School of Human Settlements and Civil Engineering, Xi'an Jiao tong University, Xi'an 710049, China
  • Corresponding Author:
    CHEN Jin (1978-), male, Ph.D., Associate Professor. E-mail:

    ZHENG Huiqi (1993-), male, Master candidate. E-mail:

出版时间: 2020-05-20 doi: 10.14062/j.issn.0454-5648.2020.05.20190429
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以Ti3C2Tx为基底材料,异丙醇(C3H8O)为诱导剂,通过溶剂热法制备TiO2/Ti3C2Tx复合材料。采用X射线衍射、扫描电子显微镜、X射线光电子能谱和紫外可见漫反射光谱对样品物相组成及微观结构进行表征。结果表明:在Ti3C2Tx层状表面均匀生长出锐钛矿晶型的TiO2,所得TiO2/Ti3C2Tx复合材料光生电子传输性能提高。TiO2/Ti3C2Tx-24 h在500 W汞灯(波长为365 nm)照射下其光催化性能最佳,75 min可降解甲基橙(MO)95%,比纯TiO2光催化剂降解效率提高了67.7%。

碳化钛  /  二氧化钛  /  复合材料  /  溶剂热法  /  光催化

TiO2/Ti3C2Tx composites were synthesized by a solvothermal method with Ti3C2Tx as substrate and isopropanol (C3H8O) as an inducer. The phase composition and microstructure of TiO2/Ti3C2Tx were characterized by X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy and ultraviolet-visible diffuse reflectance spectroscopy. The results show that anatase type TiO2 is uniformly grown on the layered surface of Ti3C2Tx, thus improving the electron transport performance of TiO2/Ti3C2Tx composites. The optimum photocatalytic performance of TiO2/Ti3C2Tx-24 h can be obtained under the irradiation of 500 W mercury lamp (365 nm UV light), and the degradation efficiency of methyl orange (MO) is 95% for 75 min, which is 67.7% greater than that of pure TiO2 photocatalyst.

titanium carbide  /  titanium dioxide  /  composite  /  solvothermal methods  /  photocatalysis
郑会奇, 陈晋, 赵杨, 王文东, 雷西萍. 溶剂热法原位制备TiO2/Ti3C2Tx复合材料及其光催化性能. 硅酸盐学报, 2020 , 48 (5) : 723 -729 . DOI: 10.14062/j.issn.0454-5648.2020.05.20190429
Huiqi ZHENG, Jin CHEN, Yang ZHAO, Wendong WANG, Xiping LEI. In-situ Solvothermal Synthesis and Photocatalytic Performance of TiO2/Ti3C2Tx Composites[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (5) : 723 -729 . DOI: 10.14062/j.issn.0454-5648.2020.05.20190429
  • 国家自然科学基金(21007050)
  • 陕西省重大科技成果转化引导专项(2016KTCG01-17)
  • 西安建筑科技大学“超级电容器电极材料设计与应用”团队建设资金
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2020年第48卷第5期
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doi: 10.14062/j.issn.0454-5648.2020.05.20190429
  • 接收时间:2019-06-24
  • 首发时间:2026-10-29
  • 出版时间:2020-05-20
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出版历史
  • 收稿日期:2019-06-24
  • 修回日期:2019-07-20
基金
国家自然科学基金(21007050)
陕西省重大科技成果转化引导专项(2016KTCG01-17)
西安建筑科技大学“超级电容器电极材料设计与应用”团队建设资金
作者信息
    1.西安建筑科技大学材料科学与工程学院,西安 710055
    2.西安交通大学人居环境与建筑工程学院,西安 710049

通讯作者:

陈晋(1978—),男,博士,副教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.2020.05.20190429
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
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属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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