Article(id=1322612421169099533, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612332010787465, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190776, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1574956800000, receivedDateStr=2019-11-29, revisedDate=1576598400000, revisedDateStr=2019-12-18, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264974157, onlineDateStr=2026-10-29, pubDate=1592582400000, pubDateStr=2020-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264974157, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264974157, creator=13701087609, updateTime=1793264974157, updator=13701087609, issue=Issue{id=1322612332010787465, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='6', pageStart='787', pageEnd='938', issueExtLink='null', onlineDate='null', pubDate='1592582400000', pubDateStr='2020-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264952900, creator='13701087609', updateTime=1793277066146, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663138810516224, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612332010787465, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663138810516225, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612332010787465, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=787, endPage=793, ext={EN=ArticleExt(id=1322612421391397646, articleId=1322612421169099533, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Aluminum Nitride Nanomaterials by Precursor Method, columnId=1322612347886228180, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Topic on Engineering Ceramic Materials, runingTitle=null, highlight=null, articleAbstract=

Al(CON₂H₄)₆Cl₃ was firstly synthesized as a precursor with urea and AlCl₃·6H₂O as a nitrogen source and an aluminum source, respectively, and then the precursor was calcined at 1 000 ℃ to prepare spherical h-AlN nanoparticles. The effects of atmosphere pressure and sintering time on the morphology and the nucleation-growth mechanism of AlN were investigated. The results show that spherical AlN particles with the sizes of 320-460 nm are formed by equiaxed fine grains of smaller than 10 nm and amorphous phase under N₂ pressure of 0.1-0.2 MPa. As the N₂ pressure increases to 0.5 MPa, the diameter of spherical AlN increases to 650 nm, and rod-shaped AlN crystals appear in the aggregates. The size and number of rod crystals increase as the sintering time increases. AlN nanoparticles are formed by the reaction of AlCl₃ and NH₃ due to the decomposition of the precursor. The gas phase saturation in the crucible increases as N₂ pressure increases, promoting the nucleation and growth of AlN, reducing the amorphous phase content, and enhancing the crystallinity of AlN.

, authors=Zixuan LI¹, Liucheng HAO^{1, 2}, Jianfei ZHANG¹, Xiaonan ZHOU¹, Xin HUANG¹, Zhongqi SHI¹, Jianfeng YANG¹, Bo WANG¹, authorsList=Zixuan LI, Liucheng HAO, Jianfei ZHANG, Xiaonan ZHOU, Xin HUANG, Zhongqi SHI, Jianfeng YANG, Bo WANG, authorCompany=null, correspAuthors=Bo WANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322612421655638799, articleId=1322612421169099533, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=前驱体法合成氮化铝纳米材料及其生长机制, columnId=1322612348045611734, journalTitle=硅酸盐学报, columnName=工程陶瓷材料专题, runingTitle=null, highlight=null, articleAbstract=

以尿素为固体氮源、AlCl₃·6H₂O为铝源，通过溶液反应合成金属络合物前驱体Al（CON₂H₄）₆Cl₃，前驱体经过1 000 ℃煅烧，制备得到球形h-AlN纳米颗粒。研究了气氛压力及合成时间对AlN纳米颗粒形貌的影响及AlN的形核生长机制。结果表明：在0.1~0.2 MPa的N₂压力下，球状AlN颗粒由<10 nm的等轴状细小晶粒与非晶相团聚而成，直径为320~460 nm；随着N₂压力增至0.5 MPa，球状AlN直径增加至650 nm，团聚体中棒状AlN晶体出现，随着烧结时间延长，棒状晶尺寸增大，数量增加。AlN纳米颗粒由前驱体分解形成的AlCl₃和NH₃反应而成，随着N₂压力增大，坩埚内气相饱和度增大，促进了AlN的形核与生长，使得非晶相含量减少，AlN结晶度提高。

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LI Zixuan (1994-), female, Master candidate. E-mail: 540821134@qq.com

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LI Zixuan (1994-), female, Master candidate. E-mail: 540821134@qq.com

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李紫璇（1994—），女，硕士研究生。

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李紫璇（1994—），女，硕士研究生。

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