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Article(id=1322636194765197858, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636152813768892, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190766, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1574697600000, receivedDateStr=2019-11-26, revisedDate=1578153600000, revisedDateStr=2020-01-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270642224, onlineDateStr=2026-10-29, pubDate=1597852800000, pubDateStr=2020-08-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270642224, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270642224, creator=13701087609, updateTime=1793270642224, updator=13701087609, issue=Issue{id=1322636152813768892, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='8', pageStart='1145', pageEnd='1352', issueExtLink='null', onlineDate='null', pubDate='1597852800000', pubDateStr='2020-08-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270632222, creator='13701087609', updateTime=1793277122165, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663373687337109, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636152813768892, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663373687337110, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636152813768892, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1325, endPage=1332, ext={EN=ArticleExt(id=1322636194958135843, articleId=1322636194765197858, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Expanded Vermiculite via Chemical-Microwave Method and Correlation Between Expansion Rate and Flexibility, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

A flexible expanded vermiculite (FEV) with a high expansion ratio was prepared by a chemical-microwave method with industrial vermiculite as a raw material. The optional process and relationship between expansion rate and flexibility were investigated. The results show that the expansion ratio of FEV prepared by chemical-microwave heating is up to 36.36. The screen tailings yield of FEV samples is negatively correlated to the expansion rate, and the sharp expansion action can improve the exfoliation ability of expanded vermiculite particles, thereby reducing the flexibility of FEV sample particles. The interior of FEV is loose and porous, the pores are evenly distributed and the intact layered structure is still maintained. The thickness of the inner wall forming the narrow slit is 50-200 nm. The FEV is a low-cost precursor of vermiculite nanomaterial, which can be mechanically exfoliated to prepare vermiculite nanomaterial based on its lamellar dissociation characteristic.

, authors=Yanyan XIE1, 2, Hongjuan SUN1, 2, 3, Tongjiang PENG1, 2, 3, 4, Liming LUO1, 2, Jingfei TIAN1, 2, authorsList=Yanyan XIE, Hongjuan SUN, Tongjiang PENG, Liming LUO, Jingfei TIAN, authorCompany=null, correspAuthors=Hongjuan SUN, authorNote=

XIE Yanyan (1994-), male, Master candidate. E-mail:

, correspAuthorsNote=
SUN Hongjuan (1976-), female, Ph.D., Professor. E-mail:
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以工业蛭石为原料，利用化学-微波法制备具有高膨胀倍数的柔性膨胀蛭石（FEV），研究FEV的最佳制备工艺及膨胀倍数与柔韧性相关性。结果表明：利用化学-微波加热法制备的FEV膨胀倍数最高达36.36倍。FEV样品的筛上产率与膨胀率呈负相关，剧烈的膨胀作用可提高膨胀蛭石颗粒的剥离性，进而降低FEV样品颗粒的柔韧性。FEV内部疏松多孔，孔隙分布较均匀，依旧保持完整的层状结构，构成狭缝状缝隙的内壁厚度为50~200 nm。FEV是一种低成本制备蛭石纳米材料的前驱体，可基于其层解充分的特性进行机械剥离，制备蛭石纳米片。

, authors=解颜岩1, 2, 孙红娟1, 2, 3, 彭同江1, 2, 3, 4, 罗利明1, 2, 田景斐1, 2, authorsList=解颜岩, 孙红娟, 彭同江, 罗利明, 田景斐, authorCompany=null, correspAuthors=孙红娟, authorNote=

解颜岩（1994—），男，硕士研究生。

, correspAuthorsNote=
孙红娟（1976—），女，博士，教授。
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XIE Yanyan (1994-), male, Master candidate. E-mail:

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XIE Yanyan (1994-), male, Master candidate. E-mail:

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解颜岩（1994—），男，硕士研究生。

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膨胀蛭石的化学-微波法制备及其膨胀率与柔韧性的关系
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解颜岩 1, 2 , 孙红娟 1, 2, 3 , 彭同江 1, 2, 3, 4 , 罗利明 1, 2 , 田景斐 1, 2
硅酸盐学报 | 研究论文 2020,48(8): 1325-1332
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硅酸盐学报 |研究论文 2020 , 48 (8) : 1325 -1332
膨胀蛭石的化学-微波法制备及其膨胀率与柔韧性的关系
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解颜岩1, 2 , 孙红娟1, 2, 3 , 彭同江1, 2, 3, 4, 罗利明1, 2, 田景斐1, 2
作者信息
  • 1．西南科技大学，固体废物处理与资源化教育部重点实验室，四川 绵阳 621010
  • 2．西南科技大学矿物材料及应用研究所，四川 绵阳 621010
  • 3．西南科技大学，四川省非金属矿粉体改性与高质化利用技术工程实验室，四川 绵阳 621000
  • 4．西南科技大学分析测试中心，四川 绵阳 621010
通讯作者:
孙红娟（1976—），女，博士，教授。
作者简介:

解颜岩（1994—），男，硕士研究生。

Preparation of Expanded Vermiculite via Chemical-Microwave Method and Correlation Between Expansion Rate and Flexibility
Yanyan XIE1, 2 , Hongjuan SUN1, 2, 3 , Tongjiang PENG1, 2, 3, 4, Liming LUO1, 2, Jingfei TIAN1, 2
Affiliations
  • 1.Key Laboratory of Ministry of Education for Solid Waste Treatment and Resource Recycle, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
  • 2.Institute of Mineral Materials and Applications, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
  • 3.Sichuan Engineering Lab of Nonmetallic Mineral Powder Modification & High-quality Utilization, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
  • 4.Center of Forecasting and Analysis, Southwest University of Science and Technology, Mianyang 621010, Sichuan, China
    • Corresponding Author:
    SUN Hongjuan (1976-), female, Ph.D., Professor. E-mail:

    XIE Yanyan (1994-), male, Master candidate. E-mail:

出版时间: 2020-08-20 doi: 10.14062/j.issn.0454-5648.20190766
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以工业蛭石为原料，利用化学-微波法制备具有高膨胀倍数的柔性膨胀蛭石（FEV），研究FEV的最佳制备工艺及膨胀倍数与柔韧性相关性。结果表明：利用化学-微波加热法制备的FEV膨胀倍数最高达36.36倍。FEV样品的筛上产率与膨胀率呈负相关，剧烈的膨胀作用可提高膨胀蛭石颗粒的剥离性，进而降低FEV样品颗粒的柔韧性。FEV内部疏松多孔，孔隙分布较均匀，依旧保持完整的层状结构，构成狭缝状缝隙的内壁厚度为50~200 nm。FEV是一种低成本制备蛭石纳米材料的前驱体，可基于其层解充分的特性进行机械剥离，制备蛭石纳米片。

草酸  /  双氧水  /  微波  /  膨胀蛭石  /  高膨胀倍数  /  柔韧性

A flexible expanded vermiculite (FEV) with a high expansion ratio was prepared by a chemical-microwave method with industrial vermiculite as a raw material. The optional process and relationship between expansion rate and flexibility were investigated. The results show that the expansion ratio of FEV prepared by chemical-microwave heating is up to 36.36. The screen tailings yield of FEV samples is negatively correlated to the expansion rate, and the sharp expansion action can improve the exfoliation ability of expanded vermiculite particles, thereby reducing the flexibility of FEV sample particles. The interior of FEV is loose and porous, the pores are evenly distributed and the intact layered structure is still maintained. The thickness of the inner wall forming the narrow slit is 50-200 nm. The FEV is a low-cost precursor of vermiculite nanomaterial, which can be mechanically exfoliated to prepare vermiculite nanomaterial based on its lamellar dissociation characteristic.

oxalic acid  /  hydrogen peroxide  /  microwave  /  expanded vermiculite  /  high expansion ratio  /  flexibility
解颜岩, 孙红娟, 彭同江, 罗利明, 田景斐. 膨胀蛭石的化学-微波法制备及其膨胀率与柔韧性的关系. 硅酸盐学报, 2020 , 48 (8) : 1325 -1332 . DOI: 10.14062/j.issn.0454-5648.20190766
Yanyan XIE, Hongjuan SUN, Tongjiang PENG, Liming LUO, Jingfei TIAN. Preparation of Expanded Vermiculite via Chemical-Microwave Method and Correlation Between Expansion Rate and Flexibility[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (8) : 1325 -1332 . DOI: 10.14062/j.issn.0454-5648.20190766
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  • 国家重点研发项目(2018YFC1802902)
  • 国家自然科学基金(41972042)
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2020年第48卷第8期
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doi: 10.14062/j.issn.0454-5648.20190766
  • 接收时间：2019-11-26
  • 首发时间：2026-10-29
  • 出版时间：2020-08-20
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  • 收稿日期：2019-11-26
  • 修回日期：2020-01-05
基金
国家重点研发项目(2018YFC1802902)
国家自然科学基金(41972042)
作者信息
    1．西南科技大学，固体废物处理与资源化教育部重点实验室，四川 绵阳 621010
    2．西南科技大学矿物材料及应用研究所，四川 绵阳 621010
    3．西南科技大学，四川省非金属矿粉体改性与高质化利用技术工程实验室，四川 绵阳 621000
    4．西南科技大学分析测试中心，四川 绵阳 621010

通讯作者:

孙红娟（1976—），女，博士，教授。
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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