Article(id=1322612312142369259, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190707, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1572192000000, receivedDateStr=2019-10-28, revisedDate=1572883200000, revisedDateStr=2019-11-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264948163, onlineDateStr=2026-10-29, pubDate=1589904000000, pubDateStr=2020-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264948163, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264948163, creator=13701087609, updateTime=1793264948163, updator=13701087609, issue=Issue{id=1322612265061306700, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='5', pageStart='615', pageEnd='786', issueExtLink='null', onlineDate='null', pubDate='1589904000000', pubDateStr='2020-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264936938, creator='13701087609', updateTime=1793276961694, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662700602208333, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662700602208334, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=745, endPage=752, ext={EN=ArticleExt(id=1322612312314335724, articleId=1322612312142369259, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Processing, Characterization and Performance of Modified Calcium Polyphosphate Prepared by Hydrothermal Method, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Calcium polyphosphate (CPP) was modified via the Schotton-Baumann acylation reaction using 12-aminododecanoic acid (12-AA) and acryloyl chloride as main raw materials. The effects of hydrothermal reaction time and 12-AA dosage on the modification process of CPP were investigated. They were characterized by Fourier infrared spectroscopy, X-ray diffraction and scanning electron microscopy. The particle size, contact angle and thermal stability of CPP were also determined. The results show that the yield of CPP-modified increases with increasing the hydrothermal reaction time and 12-AA content. In the acylation process, the pH value decreases as the reaction time increases until stable (i.e., a weak acidity, pH 6.2). A greater yield (i.e., 56.70%) and the smaller particle size (i.e., 588.3±119.7 nm) of modified CPP are obtained when a molar ratio of CPP to 12-AA is 1∶3 and the reaction time is 12 h. The contact angle before and after the modification increases from 2 to 61.41 degrees. Based on the results by thermogravimetric analysis, the CPP has a good thermal stability with little mass loss at <592.92 ℃. However, the modified CPP still has a good thermal stability and shows an obvious mass loss at 426.68-461.66 ℃.

, authors=Chen WANG, Jing LIU, Liang WANG, Sixian LU, authorsList=Chen WANG, Jing LIU, Liang WANG, Sixian LU, authorCompany=null, correspAuthors=Liang WANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322612312532439533, articleId=1322612312142369259, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=基于水热法制备改性聚磷酸钙的工艺调控、表征及性能, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以12-氨基十二烷酸（12-AA）、丙烯酰氯为主要原料，通过Schotton-Baumann酰化反应对聚磷酸钙（CPP）进行改性。探究了水热反应时间和12-AA用量对CPP改性工艺的影响，并利用Fourier红外、X射线衍射、扫描电子显微镜对产物进行了表征，同时研究了CPP的粒度、接触角和热稳定性能。结果表明：随着水热反应时间与12-AA含量的增加，CPP的产率呈增长趋势，酰化反应过程中体系pH值随反应时间的增加呈减小趋势直至平稳（呈弱酸性，pH=6.2）。当反应时间为12 h，CPP与12-AA的摩尔比为1∶3时，产率可达56.70%，粒径较小（588.3±119.7 nm）；改性前后接触角由2°提高至61.41°；未改性CPP无明显失重（分解温度为592.92 ℃），热稳定性良好。改性CPP出现明显失重，分解温度在426.68~461.66 ℃范围内，仍保持良好的热稳定性。

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WANG Chen (1963-), female, Ph.D., Professor. E-mail: wangchen2231@xpu.edu.cn

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WANG Chen (1963-), female, Ph.D., Professor. E-mail: wangchen2231@xpu.edu.cn

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王琛（1963—），女，博士，教授。

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王琛（1963—），女，博士，教授。

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