Article(id=1322612276725662463, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612228126265395, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190624, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1568131200000, receivedDateStr=2019-09-11, revisedDate=1569340800000, revisedDateStr=2019-09-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264939718, onlineDateStr=2026-10-29, pubDate=1587312000000, pubDateStr=2020-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264939718, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264939718, creator=13701087609, updateTime=1793264939718, updator=13701087609, issue=Issue{id=1322612228126265395, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='4', pageStart='463', pageEnd='614', issueExtLink='null', onlineDate='null', pubDate='1587312000000', pubDateStr='2020-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264928132, creator='13701087609', updateTime=1793276729826, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661728073138752, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612228126265395, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661728073138753, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612228126265395, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=577, endPage=583, ext={EN=ArticleExt(id=1322612278030091008, articleId=1322612276725662463, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Synthetic Methods on Synthesis of Hierarchical Porous SAPO-11, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A hierarchical porous SAPO-11 zeolite was synthesized via dodecyl trimethylammonium bromide (DTAB) as a mesoporous template and hydrochloric acid post-treatment, respectively. The synthesized samples were characterized by X-ray diffraction, N₂ adsorption-desorption, scanning electron microscopy and transmission electron microscopy. The effect of different synthetic methods on the structure and morphology of the hierarchical porous SAPO-11 was investigated. The results indicate that the content of mesoporous template DTAB has a great influence on the pore structure and external surface area of SAPO-11. When n(DTAB)∶n(Al₂O₃)=0.4∶1.0, the composition of the synthesis system is n(Al₂O₃)∶n(P₂O₅)∶n(DPA+DIPA)∶n(SiO₂)∶n(H₂O)=1.0∶1.0∶1.0∶0.5∶50.0, the external surface area and pore volume of the synthesized hierarchical pore SAPO-11 become the maximum values. For the hydrochloric acid post-treatment, the maximum external surface area and pore volume of hierarchical pore SAPO-11 are obtained when the concentration of hydrochloric acid is 0.3 mol/L. Compared to the two methods, hydrochloric acid treatment can destroy the spherical morphology of SAPO-11. Besides the slit holes produced due to the grain accumulation, the channels also come from the slit holes formed due to the layer structure. The hierarchical holes of SAPO-11 synthesized with mesoporous template DTAB mainly comes from the slit holes formed due to the grain accumulation. The crystal structure of the zeolite retains and the specific surface area increases.

, authors=Zhiping CHEN^{1, 2}, Faxiang SHI¹, Guangheng WANG¹, Wenwu ZHOU^{1, 2}, Ying QU¹, Zhiyuan YANG^{1, 2}, Anning ZHOU^{1, 2}, authorsList=Zhiping CHEN, Faxiang SHI, Guangheng WANG, Wenwu ZHOU, Ying QU, Zhiyuan YANG, Anning ZHOU, authorCompany=null, correspAuthors=Wenwu ZHOU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322612279284187905, articleId=1322612276725662463, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=合成方法对合成多级孔SAPO-11分子筛的影响, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用以十二烷基三甲基溴化铵（DTAB）作为介孔模板剂和盐酸后处理的方法分别制备了多级孔SAPO-11分子筛。利用X射线衍射、N₂吸附-脱附、扫描电子显微镜和透射电子显微镜等分析手段对2种方法合成的多级孔SAPO-11分子筛进行了表征，研究不同合成方法对多级孔SAPO-11结构、形貌等性质的影响。结果表明，介孔模板剂DTAB的含量对SAPO-11的孔结构和外表面积有较大的影响，当n（DTAB）∶n（Al₂O₃）=0.4∶1.0，原料配比为n（Al₂O₃）∶n（P₂O₅）∶n（二正丙胺+二异丙胺）∶n（SiO₂）∶n（H₂O）=1.0∶1.0∶1.0∶0.5∶50.0的条件下，合成的多级孔SAPO-11外表面积和孔体积最大；盐酸酸洗方法中，当盐酸浓度为0.3 mol/L时得到的多级孔SAPO-11外表面积和孔体积最大；2种合成方法相比，盐酸酸洗破坏了SAPO-11的球形晶貌，孔道除了来源于片状晶粒堆积产生的狭缝孔外，还来源于大量层状结构产生的狭缝孔，而以介孔模板剂合成的多级孔SAPO-11孔道主要来源于片状晶粒堆积产生的狭缝孔，更好地保留了分子筛的晶型结构，增大了比表面积。

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CHEN Zhiping (1982-), male, Ph.D., Lecturer. E-mail: cupczp@163.com

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