Article(id=1322612206202634597, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190421, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1561046400000, receivedDateStr=2019-06-21, revisedDate=1562428800000, revisedDateStr=2019-07-07, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264922904, onlineDateStr=2026-10-29, pubDate=1584633600000, pubDateStr=2020-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264922904, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264922904, creator=13701087609, updateTime=1793264922904, updator=13701087609, issue=Issue{id=1322612191723897081, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='3', pageStart='325', pageEnd='462', issueExtLink='null', onlineDate='null', pubDate='1584633600000', pubDateStr='2020-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264919452, creator='13701087609', updateTime=1793277037156, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663017125368549, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663017125368550, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=375, endPage=380, ext={EN=ArticleExt(id=1322612206391378278, articleId=1322612206202634597, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of TiN Source on Microstructures and Mechanical Properties of Hot-pressed Si₃N₄-TiN Ceramics, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The effect of TiN source (i.e., TiN powder, TiO₂ powder and TiO₂ sol) on the phase compositions, microstructures and mechanical properties of hot-pressed Si₃N₄-TiN ceramics was investigated. The results show that only β-Si₃N₄ and TiN phases are detected for the sample with TiN powder. The sizes of β-Si₃N₄ and TiN grains are large, the Vickers hardness, flexure strength, and fracture toughness are (15.6±0.3) GPa, (1 058±78) MPa, and (11.2±0.6) MPa·m^1/2, respectively. However, the O′-Sialon phase appears in the sample with TiO₂ powder in addition to β-Si₃N₄ and TiN phases, and the content of O′-Sialon is 8.7wt%. Due to the relatively fine grains of β-Si₃N₄ and TiN, the Vickers hardness increases to (16.7±0.4) GPa, and the flexure strength and fracture toughness are (986±76) MPa and (11.3±0.4) MPa·m^1/2, respectively. Moreover, the O′-Sialon phase appears in the sample with TiO₂ sol, the content of O′-Sialon is 12.5wt%, and the size of β-Si₃N₄ and TiN grains is finer, having a higher Vickers hardness (i.e., 16.6±0.5 GPa), and relatively lower flexure strength (i.e., 788±94 MPa) and fracture toughness (i.e., 10.2±1.0 MPa·m^1/2). Si₃N₄-TiN ceramics with uniformly fine microstructures and good mechanical properties can be thus obtained with TiO₂ powder.

, authors=Wanxin WEI, Junjie YU, Weijian LIU, Weiming GUO, Huatay LIN, authorsList=Wanxin WEI, Junjie YU, Weijian LIU, Weiming GUO, Huatay LIN, authorCompany=null, correspAuthors=Weiming GUO, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322612206634647911, articleId=1322612206202634597, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=TiN对热压烧结Si₃N₄-TiN复相陶瓷显微结构和力学性能的影响, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

研究了TiN的来源（TiN粉、TiO₂粉和TiO₂溶胶）对热压烧结Si₃N₄-TiN复相陶瓷的相组成、显微结构与力学性能的影响。结果表明，当以TiN粉为第二相添加剂时，试样中仅检测到β-Si₃N₄和TiN相，Si₃N₄晶粒与TiN颗粒较粗大，硬度、强度和断裂韧性分别为（15.6±0.3）GPa、（1 058±78）MPa和（11.2±0.6）MPa·m^1/2；当以TiO₂粉为第二相添加剂时，除了β-Si₃N₄和TiN相，还检测到O′-Sialon相，O′-Sialon相的含量为8.7%（质量分数），Si₃N₄晶粒与TiN颗粒均匀细小，样品硬度提高到（16.7±0.4）GPa，强度和断裂韧性没有显著变化，分别为（986±76）MPa和（11.3±0.4）MPa·m^1/2；当以TiO₂溶胶为第二相添加剂时，同样检测到O′-Sialon相，O′-Sialon相的含量为12.5%，Si₃N₄晶粒与TiN颗粒均匀细小，样品硬度较高为（16.6±0.5）GPa，其强度和断裂韧性较低分别为（788±94）MPa和（10.2±1.0）MPa·m^1/2。以TiO₂粉为第二相添加剂时，可获得显微结构均匀细化、综合力学性能较佳的Si₃N₄-TiN复相陶瓷材料。

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WEI Wanxin (1994-), male, Master candidate. E-mail: 874955365@qq.com

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魏万鑫（1994—），男，硕士研究生。

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魏万鑫（1994—），男，硕士研究生。

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