Article(id=1322608958737592753, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190317, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1557763200000, receivedDateStr=2019-05-14, revisedDate=1562256000000, revisedDateStr=2019-07-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264148648, onlineDateStr=2026-10-29, pubDate=1579449600000, pubDateStr=2020-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264148648, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264148648, creator=13701087609, updateTime=1793264148648, updator=13701087609, issue=Issue{id=1322608929100649011, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='1', pageStart='1', pageEnd='146', issueExtLink='null', onlineDate='null', pubDate='1579449600000', pubDateStr='2020-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264141583, creator='13701087609', updateTime=1793276771816, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661904204542961, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661904208737266, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1, endPage=7, ext={EN=ArticleExt(id=1322608959630979506, articleId=1322608958737592753, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Electrospray Preparation and Microwave Absorption Properties of La³⁺-doped SnO₂ Hollow Micro/nanospheres, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

La³⁺-doped SnO₂ hollow micro/nanospheres were prepared by electrospray and calcination techniques with lanthanum nitrate, stannous chloride and polyvinylpyrrolidone (PVP) as raw materials. The formation mechanism of hollow structure was analyzed. The crystalline phase and micromorphology of the samples were examined by thermal gravimetric analysis (TGA), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM). The microwave absorption properties of La³⁺-doped SnO₂ were determined by a vector network analyzer. The results show that La³⁺-doped SnCl₂/PVP precursor polymer appears smooth spheres with the diameters of 0.5-2.2 μm. The pure rutile structure of SnO₂ forms at 600 ℃, and La³⁺ doping does not change the crystal structure. La³⁺-doped SnO₂ micro/nanospheres appear to be a hollow structure, and the surfaces are made up of massive small particles. The optimum microwave absorption properties of La³⁺-doped SnO₂ hollow micro/nanospheres with the matching thickness of 2 mm can be obtained when the doping ratio of La³⁺ is 0.6% (in mole). The minimum reflectivity can reach -29 dB at 11.1 GHz, and the frequency band with a reflectivity less than -10 dB is 10.0-13.0 GHz. When the doping ratio of La³⁺ is 0.6%, the minimum reflectivity of La³⁺-doped SnO₂ hollow micro/nanospheres shifts to a low frequency as the matching thickness increases. The matching thickness is 4 mm at lower than 8 GHz, thus obtaining the optimum microwave absorption properties. The minimum reflectivity can reach -27 dB at 4.9 GHz, and the frequency band with a reflectivity less than -10 dB is 4.5-5.8 GHz.

, authors=Fang ZHAO, Sa ZHANG, Xiangjun TANG, Zhaogang CHENG, Kai HAN, authorsList=Fang ZHAO, Sa ZHANG, Xiangjun TANG, Zhaogang CHENG, Kai HAN, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608960406925747, articleId=1322608958737592753, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=镧掺杂二氧化锡中空微纳米球的制备及吸波性能, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以硝酸镧、氯化亚锡和聚乙烯吡咯烷酮（PVP）为原料，采用电喷法结合后续高温煅烧技术制备了La³⁺掺杂SnO₂中空微纳米球。通过热重分析仪、Fourier变换红外光谱仪、X射线衍射仪、扫描电子显微镜和矢量网络分析仪等手段对目标产物进行了表征，研究了SnO₂微纳米球中空结构的形成机制及La³⁺掺杂对其物相、微观形貌和吸波性能的影响。研究表明：La³⁺掺杂SnCl₂/PVP前驱体聚合物呈完整球形，表面光滑，球径分布在0.5~2.2 μm之间。经600 ℃煅烧后，均生成了单一金红石型SnO₂，且La³⁺的加入未改变SnO₂的晶体结构；煅烧后产物均为中空球状，球面由许多小颗粒堆积而成，表面粗糙不平。当匹配厚度为2 mm时，La³⁺掺杂比例为0.6%（摩尔分数）的产物的吸波效果最佳：最低反射率为-29 dB，对应的吸收频率为11.1 GHz，低于-10 dB的吸收频带为10.0~13.0 GHz；该掺杂比例的产物随匹配厚度增加，最低反射率向低频移动，在8 GHz以下的最佳匹配厚度为4 mm，在此厚度下吸波性能优良：最低反射率为-27 dB，对应的吸收频率为4.9 GHz，低于-10 dB的吸收频带为4.5~5.8 GHz。

, authors=赵芳, 张飒, 唐香珺, 程兆刚, 韩凯, authorsList=赵芳, 张飒, 唐香珺, 程兆刚, 韩凯, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=DVp/y24MShAdY5V38lWFQw==, magXml=USpEwzXTUyKmINilp/JckQ==, pdfUrl=null, pdf=VxSAdIK62fBbqXtFHPfO6g==, pdfFileSize=1829922, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=HNetibC/WIk922Hkd33l0w==, mapNumber=null, fund=null)}, authors=[Author(id=1322954620489835354, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322608958737592753, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=zhaofang19821106@163.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1322954620556944220, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322608958737592753, authorId=1322954620489835354, language=EN, stringName=Fang ZHAO, firstName=Fang, middleName=null, lastName=ZHAO, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=Shijiazhuang Campus of Army Engineering University, Shijiazhuang 050003, China, bio={"content":"

ZHAO Fang (1982-), famale, Master, Associate Professor. E-mail: zhaofang19821106@163.com

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ZHAO Fang (1982-), famale, Master, Associate Professor. E-mail: zhaofang19821106@163.com

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赵芳（1982—），女，硕士，副教授。

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赵芳（1982—），女，硕士，副教授。

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