Article(id=1322608962114011575, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190231, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1554912000000, receivedDateStr=2019-04-11, revisedDate=1558281600000, revisedDateStr=2019-05-20, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264149453, onlineDateStr=2026-10-29, pubDate=1579449600000, pubDateStr=2020-01-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264149453, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264149453, creator=13701087609, updateTime=1793264149453, updator=13701087609, issue=Issue{id=1322608929100649011, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='1', pageStart='1', pageEnd='146', issueExtLink='null', onlineDate='null', pubDate='1579449600000', pubDateStr='2020-01-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264141583, creator='13701087609', updateTime=1793276771816, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661904204542961, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661904208737266, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608929100649011, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=61, endPage=64, ext={EN=ArticleExt(id=1322608962399224248, articleId=1322608962114011575, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Characterization of Mid-infrared Hot-melt Laser Ceramic Powders, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Tm, Ho:Gd₃Ga₅O₁₂ (Tm, Ho:GGG) nanopowders were synthesized via the sol-gel method. Tm, Ho:GGG ultrafine powders were synthesized by using Ga(NO₃)₃ and Gd(NO₃)₃ as raw materials and by replacing Gd with certain amounts of Tm and Ho. The phase structure, thermal stability, particle size, and morphology of the Tm, Ho:GGG ultrafine powers were analyzed by X-ray diffraction, infrared spectroscopy, scanning electron microscopy, thermogravimetry-differential thermal analysis, and fluorescence spectroscopy. The results revealed that a pure GGG phase was obtained after the calcination of Tm, Ho:GGG at 900 ℃, and the obtained nanopowder had a uniform particle size of 70-90 nm, good dispersibility, and fluidity. The fluorescence analysis determined that the strongest peak of the fluorescence emission spectrum was at 1 950 nm, which was associated with the ⁵I₇→⁵I₈ transition of Ho³⁺.

, authors=Xuejian ZHANG^{1, 2}, Chenyang XIA^{1, 2}, Shoufeng ZHANG^{1, 2}, Chun LI³, Huisheng LIU^{1, 2}, Yongtao LI^{1, 2}, Yimin YANG¹, Aochen DU¹, authorsList=Xuejian ZHANG, Chenyang XIA, Shoufeng ZHANG, Chun LI, Huisheng LIU, Yongtao LI, Yimin YANG, Aochen DU, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322608962848014777, articleId=1322608962114011575, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=中红外热熔激光陶瓷粉体制备与性能表征, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

通过溶胶-凝胶法合成Tm,Ho：Gd₃Ga₅O₁₂（Tm,Ho：GGG）纳米粉体，以Ga（NO₃）₃和Gd（NO₃）₃为原料，并用一定量的Tm和Ho取代Gd，合成了Tm,Ho：GGG超细粉体。借助X射线衍射、红外光谱、扫描电子显微镜、热重分析及荧光光谱技术分析了Tm,Ho：GGG超细粉的相结构，热稳定性，粒径和形貌。结果表明：Tm,Ho：GGG在900 ℃煅烧后获得粒径均匀，分散性和流动性好的GGG纯相纳米粉末，尺寸在70~90 nm之间。荧光发射的最强峰位于1950 nm，是由Ho³⁺的⁵I₇→⁵I₈转变产生。

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ZHANG Xuejian (1975-), male, Ph.D., Professor. E-mail: 357169750@qq.com

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ZHANG Xuejian (1975-), male, Ph.D., Professor. E-mail: 357169750@qq.com

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张学建（1975—），男，博士，教授。

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张学建（1975—），男，博士，教授。

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